Synthesis and characterization of p-t-butyl calix[4]crown-4 and its double calix[4]arene dimer

被引：8

作者：

Asfari, Z

Thuéry, P

Nierlich, M

Vicens, J

机构：

[1] CNRS, UMR 7512, ULP, ECPM, F-67008 Strasbourg, France

[2] CEA Saclay, SCM CNRS URA 331, F-91191 Gif Sur Yvette, France

来源：

AUSTRALIAN JOURNAL OF CHEMISTRY | 1999年 / 52卷 / 05期

关键词：

D O I：

10.1071/CH98167

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The preparation, separation, characterization and crystal structure determinations of the 1+1 and 2+2 condensation products, p-t-butyl calix[4]crown-4 (1) and its dimer double calix[4]arene double crown-4 (2), resulting from the reaction of p-t-butylcalix[4]arene with triethylene glycol ditosylate in the presence of a base are reported.

引用

页码：343 / 349

页数：7

共 23 条

[11] A novel type of double-calixcrown: Spirobiscalix[4]crowns [J].

Li, JS ;

Zhong, ZL ;

Chen, YY ;

Lu, XR .

TETRAHEDRON LETTERS, 1998, 39 (36) :6507-6510

[12] Synergistic extractions of alkali ions by p-tert-butylcalix[4] arene and crown ether mixtures [J].

Natatou, I ;

Burgard, M ;

Asfari, Z ;

Vicens, J .

JOURNAL OF INCLUSION PHENOMENA AND MOLECULAR RECOGNITION IN CHEMISTRY, 1995, 22 (02) :107-117

[13] Processing of X-ray diffraction data collected in oscillation mode [J].

Otwinowski, Z ;

Minor, W .

MACROMOLECULAR CRYSTALLOGRAPHY, PT A, 1997, 276 :307-326

[14] THE DISCOVERY OF CROWN ETHERS (NOBEL LECTURE) [J].

PEDERSEN, CJ .

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 1988, 27 (08) :1021-1027

[15] A double calix[4]arene in a 1,3-alternate conformation [J].

PerezAdelmar, JA ;

Abraham, H ;

Sanchez, C ;

Rissanen, K ;

Prados, P ;

deMendoza, J .

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION IN ENGLISH, 1996, 35 (09) :1009-1011

[16]

SAHLI C, 1992, ANALUSIS, V20, P351

[17] Calix[4]tube: A tubular receptor with remarkable potassium ion selectivity [J].

Schmitt, P ;

Beer, PD ;

Drew, MGB ;

Sheen, PD .

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION IN ENGLISH, 1997, 36 (17) :1840-1842

[18]

SHELDRICK GM, 1997, SHELXTL VERSION 5 03

[19]

SHELDRICK GM, 1990, SHELXS86 PROGRAM SOL

[20]

Vicens J., 1991, CALIXARENES VERSATIL, V3

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