学术探索
学术期刊
新闻热点
数据分析
智能评审

Purification of single-wall carbon nanotubes synthesized from alcohol by catalytic chemical vapor deposition

被引：22
作者：
Okubo, S
Sekine, T
Suzuki, S
Achiba, Y
Tsukagoshi, K
Aoyagi, Y
Kataura, H
机构：
[1] Tokyo Metropolitan Univ, Grad Sch Sci, Dept Phys, Hachioji, Tokyo 1920397, Japan
[2] Tokyo Metropolitan Univ, Grad Sch Sci, Dept Chem, Hachioji, Tokyo 1920397, Japan
[3] RIKEN, Wako, Saitama 3510198, Japan
来源：
JAPANESE JOURNAL OF APPLIED PHYSICS PART 2-LETTERS | 2004年 / 43卷 / 3B期
关键词：
carbon nanotube; purification; Raman spectroscopy; transmission electron microscopy; chemical vapor deposition; zeolite;
D O I：
10.1143/JJAP.43.L396
中图分类号：
O59 [应用物理学];
学科分类号：
摘要：
The purification of single-wall carbon nanotubes synthesized by alcohol catalytic chemical vapor deposition (ACCVD) was performed for the first time. Subsequent use of aqueous solutions of sodium hydroxide and hydrochloric acid. removed the main impurities, such as the support zeolite and the catalyst metal particles, from the as-grown material. The obtained. samples were characterized by transmission electron microscopy (TEM), thermogravimetric analysis (TGA), and Raman spectroscopy. The present purification protocol has some advantages, in terms of cost, safety, and large applicability for other carbon materials formed on zeolite.
引用
收藏
页码：L396 / L398
页数：3
相关论文
共 20 条
[1]   Bulk morphology and diameter distribution of single-walled carbon nanotubes synthesized by catalytic decomposition of hydrocarbons [J].
Cheng, HM ;
Li, F ;
Sun, X ;
Brown, SDM ;
Pimenta, MA ;
Marucci, A ;
Dresselhaus, G ;
Dresselhaus, MS .
CHEMICAL PHYSICS LETTERS, 1998, 289 (5-6) :602-610
[2]   Controllable growth of single wall carbon nanotubes by pyrolizing acetylene on the floating iron catalysts [J].
Ci, LJ ;
Xie, SS ;
Tang, DS ;
Yan, XQ ;
Li, YB ;
Liu, ZQ ;
Zou, XP ;
Zhou, WY ;
Wang, G .
CHEMICAL PHYSICS LETTERS, 2001, 349 (3-4) :191-195
[3]  
Dillon AC, 1999, ADV MATER, V11, P1354, DOI 10.1002/(SICI)1521-4095(199911)11:16<1354::AID-ADMA1354>3.0.CO
[4]  
2-N
[5]   Synthesis of single-walled carbon nanotubes using binary (Fe, Co, Ni) alloy nanoparticles prepared in situ by the reduction of oxide solid solutions [J].
Flahaut, E ;
Govindaraj, A ;
Peigney, A ;
Laurent, C ;
Rousset, A ;
Rao, CNR .
CHEMICAL PHYSICS LETTERS, 1999, 300 (1-2) :236-242
[6]   Catalytic growth of single-wall carbon nanotubes from metal particles [J].
Hafner, JH ;
Bronikowski, MJ ;
Azamian, BR ;
Nikolaev, P ;
Rinzler, AG ;
Colbert, DT ;
Smith, KA ;
Smalley, RE .
CHEMICAL PHYSICS LETTERS, 1998, 296 (1-2) :195-202
[7]   Optical properties of single-wall carbon nanotubes [J].
Kataura, H ;
Kumazawa, Y ;
Maniwa, Y ;
Umezu, I ;
Suzuki, S ;
Ohtsuka, Y ;
Achiba, Y .
SYNTHETIC METALS, 1999, 103 (1-3) :2555-2558
[8]   Diameter control of single-walled carbon nanotubes [J].
Kataura, H ;
Kumazawa, Y ;
Maniwa, Y ;
Ohtsuka, Y ;
Sen, R ;
Suzuki, S ;
Achiba, Y .
CARBON, 2000, 38 (11-12) :1691-1697
[9]   Chemical vapor deposition of methane for single-walled carbon nanotubes [J].
Kong, J ;
Cassell, AM ;
Dai, HJ .
CHEMICAL PHYSICS LETTERS, 1998, 292 (4-6) :567-574
[10]   Synthesis of individual single-walled carbon nanotubes on patterned silicon wafers [J].
Kong, J ;
Soh, HT ;
Cassell, AM ;
Quate, CF ;
Dai, HJ .
NATURE, 1998, 395 (6705) :878-881
12