Natural abundance 33S NMR spectroscopy.: The first spectra of several major compound types

被引:14
作者
Aitken, RA [1 ]
Arumugam, S [1 ]
Mesher, STE [1 ]
Riddell, FG [1 ]
机构
[1] Univ St Andrews, Sch Chem, St Andrews KY16 9ST, Fife, Scotland
来源
JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 2 | 2002年 / 02期
关键词
D O I
10.1039/b109478e
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
Using a high field, high power instrument, S-33 NMR spectra have been obtained for several previously unobservable compound types including an aromatic isothiocyanate, a thiocyanate, a thiophenol, an alkyl aryl sulfide, a thiazole, a persulfate, a sulfinic acid and sulnate salts, a sulfonhydrazide and a sulfinyl halide. The range of data for sulfonyl fluorides and chlorides has also been extended considerably.
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收藏
页码:225 / 226
页数:2
相关论文
共 17 条
[1]   Flash vacuum pyrolysis of stabilised phosphorus ylides.: Part 13.: Extrusion of Ph3P from sulfinyl ylides and reactivity of the resulting sulfinyl carbenes [J].
Aitken, RA ;
Drysdale, MJ ;
Ryan, BM .
JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1, 1998, (20) :3345-3348
[2]   Synthesis and pyrolytic behaviour of chiral thiazolidine 1,1-dioxides [J].
Aitken, RA ;
Mesher, STE .
JOURNAL OF CHEMICAL RESEARCH-S, 1998, (02) :76-77
[3]   Synthesis and pyrolytic behaviour of thiazolidin-2-one 1,1-dioxides [J].
Aitken, RA ;
Armstrong, DP ;
Galt, RHB ;
Mesher, STE .
JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1, 1997, (14) :2139-2145
[4]   Synthesis and oxidation of chiral 2-thiazolines (4,5-dihydro-1,3-thiazoles) [J].
Aitken, RA ;
Armstrong, DP ;
Galt, RHB ;
Mesher, STE .
JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1, 1997, (06) :935-943
[5]   Flash vacuum pyrolysis of stabilised phosphorus ylides.: Part 12.: Extrusion of Ph3P from sulfonyl ylides and reactivity of the resulting sulfonyl carbenes [J].
Aitken, RA ;
Drysdale, MJ ;
Ferguson, G ;
Lough, AJ .
JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1, 1998, (05) :875-880
[6]  
AITKEN RA, 1998, J CHEM RES M, P564
[7]   S-33 CHEMICAL-SHIFTS AND LINE WIDTHS OF SELECTED SULFONES, SULFOXIMIDES, SULFIMIDES, SULFIDES AND SULFONIUM IONS [J].
ANNUNZIATA, R ;
BARBARELLA, G .
ORGANIC MAGNETIC RESONANCE, 1984, 22 (04) :250-254
[8]   S-33 AND O-17 NMR OF COMPOUNDS CONTAINING THE SO2 MOIETY - A GENERALIZATION OF THE CHLORINE EFFECT [J].
BARBARELLA, G ;
CHATGILIALOGLU, C ;
TUGNOLI, V .
JOURNAL OF MAGNETIC RESONANCE, 1990, 88 (02) :277-283
[9]   S-33 AND O-17 NMR OF COMPOUNDS CONTAINING THE SO2 MOIETY - THE CHLORINE EFFECT [J].
BARBARELLA, G ;
CHATGILIALOGLU, C ;
ROSSINI, S ;
TUGNOLI, V .
JOURNAL OF MAGNETIC RESONANCE, 1986, 70 (02) :204-212
[10]   S-33 NMR OF CYCLIC SULFIDES, SULFOXIDES, AND SULFONES [J].
BARBARELLA, G ;
BONGINI, A ;
CHATGILIALOGLU, C ;
ROSSINI, S ;
TUGNOLI, V .
JOURNAL OF ORGANIC CHEMISTRY, 1987, 52 (17) :3857-3860