Microwave-assisted N-Boc deprotection under mild basic conditions using K3PO4•H2O in MeOH

被引：23

作者：

Dandepally, Srinivasa Reddy ^{[1
]}

Williams, Alfred L. ^{[1
]}

机构：

[1] N Carolina Cent Univ, Dept Pharmaceut Sci, BRITE, Durham, NC 27707 USA

来源：

TETRAHEDRON LETTERS | 2009年 / 50卷 / 09期

关键词：

CERIC AMMONIUM-NITRATE; SELECTIVE DEPROTECTION; PROTECTING GROUP; BUTOXYCARBONYL GROUP; AMINO-ACIDS; REMOVAL; DERIVATIVES; PYRROLES; INDOLES;

D O I：

10.1016/j.tetlet.2008.12.074

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

A simple and efficient method for the deprotection of secondary Boc-protected amino Compounds under mild basic conditions using K3PO4 center dot H2O in MeOH assisted by microwave irradiation has been presented. (c) 2008 Elsevier Ltd. All rights reserved.

引用

页码：1071 / 1074

页数：4

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