Three-Dimensional Visualization of Defects Formed during the Synthesis of Metal-Organic Frameworks: A Fluorescence Microscopy Study

被引：130

作者：

Ameloot, Rob ^{[1
]}

Vermoortele, Frederik ^{[1
]}

Hofkens, Johan ^{[2
]}

De Schryver, Frans C. ^{[2
]}

De Vos, Dirk E. ^{[1
]}

Roeffaers, Maarten B. J. ^{[1
]}

机构：

[1] Katholieke Univ Leuven, Ctr Surface Chem & Catalysis, B-3001 Louvain, Belgium

[2] Katholieke Univ Leuven, Dept Chem, B-3001 Louvain, Belgium

来源：

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION | 2013年 / 52卷 / 01期

基金：

欧洲研究理事会;

关键词：

crystal growth; fluorescence; fluorescence microscopy; metal-organic frameworks; microporous materials; ATOMIC-FORCE MICROSCOPY; ACID CATALYSIS; ZSM-5; CRYSTALS; ADSORPTION; ZEOLITES; FTIR; MOFS; FUNCTIONALIZATION; CRYSTALLIZATION; DIFFRACTION;

D O I：

10.1002/anie.201205627

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Imperfections in the spotlight: Fluorescence microscopy was used to detect defects in metal-organic frameworks formed during synthesis. In contrast to currently available techniques, confocal fluorescence microscopy offers the advantage of three-dimensional imaging at the single-crystal level combined with the sensitivity required to study the start of defect formation. © 2013 Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim.

引用

页码：401 / 405

页数：5

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