Linear cyclodextrin-poly(vinylamine): Synthesis and NMR characterization

被引：21

作者：

Crini, G

Torri, G

Guerrini, M

Martel, B

Lekchiri, Y

Morcellet, M

机构：

[1] UNIV SCI & TECH LILLE FLANDRES ARTOIS,LAB CHIM MACROMOL,CNRS,URA 351,F-59655 VILLENEUVE DASCQ,FRANCE

[2] IST SCI CHIM & BIOCHIM G RONZONI,I-20133 MILAN,ITALY

[3] UNIV MOHAMED 1,FAC SCI,DEPT BIOL,BIOCHIM LAB,OUJDA 6000,MOROCCO

来源：

EUROPEAN POLYMER JOURNAL | 1997年 / 33卷 / 07期

关键词：

D O I：

10.1016/S0014-3057(96)00169-3

中图分类号：

O63 [高分子化学（高聚物）];

学科分类号：

070305 ; 080501 ; 081704 ;

摘要：

The synthesis of polymers containing beta-cyclodextrin (beta-CD) residues on the side chain is described. Several cyclodextrin-poly(vinylamine) with various degrees of substitution were synthesized, using the mono-tosyl derivative of beta-cyclodextrin as reagent. Several factors (reaction time, amounts of the reactants, composition of the solvent) have been studied. A characterization was carried out using D-2 H-1 - H-1 correlation spectroscopy (COSY-TOCSY) and D-2 H-1 - C-13 heteronuclear correlation (HMQC). (C) 1997 Elsevier Science Ltd.

引用

页码：1143 / 1151

页数：9

共 19 条

[1] PREPARATION OF A POROUS MICROPARTICULATE ANION-EXCHANGE CHROMATOGRAPHY SUPPORT FOR PROTEINS [J].