A convenient hydrothermal route to mineral Ag3CuS2 nanorods

被引：31

作者：

Hu, JQ

Deng, B

Zhang, WX

Tang, KB

Qian, YT

机构：

[1] Univ Sci & Technol China, Struct Res Lab, Hefei 230026, Peoples R China

[2] Univ Sci & Technol China, Dept Chem, Hefei 230026, Peoples R China

来源：

INTERNATIONAL JOURNAL OF INORGANIC MATERIALS | 2001年 / 3卷 / 07期

关键词：

hydrothermal; Ag3CuS2; nanorods;

D O I：

10.1016/S1466-6049(01)00163-5

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

A convenient hydrothermal route is proposed for synthesizing mineral Ag3CuS2 nanorods. X-ray powder diffraction (XRD) patterns indicated the formation of Ag3CuS2, and elemental analysis and X-ray photoelectron spectra (XPS) revealed the stoichiometric relation between Ag, Cu, and S. Transmission electron microscope (TEM) images demonstrated that the final product consisted of nanorods with diameters from 30 to 150 nm and lengths from 200 mn to 1 mum. A possible formation mechanism of Ag3CuS2 nanorods was proposed. (C) 2001 Elsevier Science Ltd. All rights reserved.

引用

页码：639 / 642

页数：4

共 16 条

[1] CRYSTAL-STRUCTURE DETERMINATION OF AG3CUS2 FROM POWDER X-RAY-DIFFRACTION DATA
BAKER, CL
LINCOLN, FJ
JOHNSON, AWS
[J]. AUSTRALIAN JOURNAL OF CHEMISTRY, 1992, 45 (09) : 1441 - 1449
[2] BREITHAUPT C, 1858, BERG HUTTENMANN Z, V17, P85
[3] AN X-RAY STUDY ON THE SYSTEM AG-CU-S
DJURLE, S
[J]. ACTA CHEMICA SCANDINAVICA, 1958, 12 (07): : 1427 - 1436
[4] GRYBECK D, 1968, AM MINERAL, V53, P1530
[5] FORMATION OF MIXED COPPER(II) SULFIDE SILVER(I) SULFIDE MEMBRANES FOR COPPER(II)-SELECTIVE ELECTRODES
HEIJNE, GJM
VANDERLINDEN, WE
DENBOEF, G
[J]. ANALYTICA CHIMICA ACTA, 1977, 89 (02) : 287 - 296
[6] PREPARATION AND STUDY OF SULFIDE THIN-FILMS DEPOSITED BY THE DIP TECHNIQUE
KARANJAI, MK
DASGUPTA, D
[J]. THIN SOLID FILMS, 1987, 155 (02) : 309 - 315
[7] Chemical solution routes to single-crystal thin films
Lange, FF
[J]. SCIENCE, 1996, 273 (5277) : 903 - 909
[8] Marco R., 1992, ANAL CHEM, V64, P594
[9] Moom J., 1997, J MATER RES, V12, P189
[10] HYDROTHERMAL SYNTHESIS OF MANGANESE ZINC FERRITES
ROZMAN, M
DROFENIK, M
[J]. JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 1995, 78 (09) : 2449 - 2455

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