An innovative fabrication of nano-HA coatings on Ti-CaP nanocomposite layer using a combination of friction stir processing and electrophoretic deposition
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Farnoush, Hamidreza
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Sadeghi, Ali
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Bastami, Ashkan Abdi
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Amirkabir Univ Technol, Dept Min & Met Engn, Tehran, IranAmirkabir Univ Technol, Dept Min & Met Engn, Tehran, Iran
Bastami, Ashkan Abdi
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Moztarzadeh, Fathollah
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Mohandesi, Jamshid Aghazadeh
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Amirkabir Univ Technol, Dept Min & Met Engn, Tehran, IranAmirkabir Univ Technol, Dept Min & Met Engn, Tehran, Iran
Mohandesi, Jamshid Aghazadeh
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[1] Amirkabir Univ Technol, Dept Min & Met Engn, Tehran, Iran
In the present study, a combination of friction stir processing and electrophoretic deposition was used to fabricate nano-hydroxyapatite coatings on the Ti-CaP nanocomposite surface layer. A constant tool rotation rate of 250 rpm, travel speed of 16 mm/min and plunge depth of 1.2 mm with a tool tilt angle of 3 degrees were used to incorporate nano-hydroxyapatite particles into Ti-6Al-4V substrates. Microstructure of the stir zone was analyzed using optical and scanning electron microscopy. Microhardness profile and AFM analysis of substrates were then studied. The electrophoretic deposition of nano-HA particles was carried out at constant voltage of 30 V after 60 s. The as-deposited nano-HA coating was characterized employing scanning electron microscope and X-ray diffraction. The results of adhesion test and potentiodynamic polarization measurements showed that Ti-CaP nanocomposite layer could effectively increase the bonding strength between coating and substrate as well as corrosion resistance. (C) 2012 Elsevier Ltd and Techna Group S.r.l. All rights reserved.