Automated gel permeation chromatographic clean-up of human adipose tissue for multiresidue analysis of organochlorine compounds

被引:9
作者
Pauwels, A
David, F
Schepens, P
Sandra, P
机构
[1] Univ Instelling Antwerp, Toxicol Ctr Pharmaceut Sci, B-2610 Wilrijk, Belgium
[2] Res Inst Chromatog, B-8500 Kortrijk, Belgium
[3] State Univ Ghent, Dept Organ Chem, B-9000 Ghent, Belgium
关键词
adipose tissue; electron capture detector; gel permeation chromatography; organochlorine pesticides; polychlorinated biphenyls;
D O I
10.1080/03067319908032661
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
Human adipose tissue samples have been analysed for organochlorine pesticides and polychlorinated biphenyls (PCBs). Following a micro liquid-solid extraction, clean-up is performed by automated gel permeation chromatography. The GPC separation provides clean extracts, allowing subsequential analysis by capillary gas chromatography-electron capture detection without additional clean-up.
引用
收藏
页码:171 / 178
页数:8
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