Controlled synthesis of colloidal silver nanoparticles in capillary micro-flow reactor

被引:31
作者
He, Sheng Tai [1 ,2 ,3 ]
Liu, Yu Lan [3 ]
Maeda, Hideaki [2 ]
机构
[1] CIC BiomaGUNE, San Sebastian 20009, Spain
[2] Natl Inst Adv Ind Sci & Technol, Saga 8410052, Japan
[3] Coll Chem Biol & Mat Sci, E China Inst Technol, Fuzhou 344000, Jiangxi, Peoples R China
关键词
Micro-flow reactor; Capillary tube; Silver; Nanoparticles; Synthesis; Nanomanufacturing;
D O I
10.1007/s11051-008-9509-6
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
In this study, using a polytetrafluoroethylene (PTFE) capillary tube as a micro-flow reactor, well-dispersed colloidal silver nanoparticles were controllably synthesized with different flow rates of precursory solution. Scanning transmission electron microscopy images and UV-visible absorbance spectra showed that silver nanoparticles with large size can be prepared with slow flow rate in the PTFE capillary reactor. The effects of tube diameters on the growth of colloidal silver nanoparticles were investigated. Experiment results demonstrated that using tube with small diameter was more propitious for the controllable synthesis of silver nanoparticles with different sizes.
引用
收藏
页码:209 / 215
页数:7
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