Preparation and characterization of rectangular tin dioxide microtubes

被引:26
作者
Duan, JH [1 ]
Cao, QQ [1 ]
Yang, SG [1 ]
Huang, HB [1 ]
Zhao, XN [1 ]
Zhang, R [1 ]
Cheng, GX [1 ]
机构
[1] Nanjing Univ, Natl Lab Microstruct, Nanjing 210093, Peoples R China
基金
中国国家自然科学基金;
关键词
crystal morphology; oxides; electron back scattering diffraction;
D O I
10.1016/j.jcrysgro.2005.10.135
中图分类号
O7 [晶体学];
学科分类号
0702 [物理学]; 070205 [凝聚态物理]; 0703 [化学]; 080501 [材料物理与化学];
摘要
Rutile phase SnO2 microtubes were successfully synthesized using a thermal evaporation method at 1550 degrees C. The products were characterized by X-ray diffraction, scanning electron microscopy and micro-Raman scattering. The microtubes are as long as about 1 mm with almost perfect rectangular cross-section. They possess a large cavity channel of about 30 mu m in width and four smooth side surfaces. The side surfaces of SnO2 microtubes are (110) and (110) planes, while their tube axes are [001]. The possible formation mechanism of the rectangular SnO2 microtubes is presented. (c) 2005 Elsevier B.V. All rights reserved.
引用
收藏
页码:164 / 167
页数:4
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