An X-ray diffraction study of epitaxial TiN/NbN superlattices

被引:41
作者
Madan, A [1 ]
Yashar, P [1 ]
Shinn, M [1 ]
Barnett, SA [1 ]
机构
[1] NORTHWESTERN UNIV,DEPT MAT SCI & ENGN,EVANSTON,IL 60208
基金
美国国家科学基金会;
关键词
X-ray diffraction; superlattices; nitrides;
D O I
10.1016/S0040-6090(97)00023-0
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
X-ray diffraction measurements and simulations were carried out to characterize the composition modulation and structure of TiN/NbN superlattices. A trapezoidal/sawtooth form of the composition wave was assumed. Random d-spacing fluctuations with Gaussian width approximately 0.002 nm and layer thickness variations of 0.1-0.5 nm were incorporated to match the observed broadening of the peaks. Best fits to the experimental data showed that considerable interdiffusion was present, with up to 15 at.% metal substitution within the layers and interface widths of 0.4-2.0 nm. The interface width values agreed well with those used in hardness enhancement calculations for epitaxial TiN/NbN superlattices. (C) 1997 Elsevier Science S.A.
引用
收藏
页码:147 / 154
页数:8
相关论文
共 19 条
[1]   MODEL OF SUPERLATTICE YIELD STRESS AND HARDNESS ENHANCEMENTS [J].
CHU, X ;
BARNETT, SA .
JOURNAL OF APPLIED PHYSICS, 1995, 77 (09) :4403-4411
[2]   INFLUENCE OF STATIC ATOMIC DISPLACEMENTS ON DIFFUSE INTENSITY SCATTERED BY SOLID SOLUTIONS [J].
COOK, HE .
JOURNAL OF PHYSICS AND CHEMISTRY OF SOLIDS, 1969, 30 (05) :1097-&
[3]   STRUCTURAL REFINEMENT OF SUPERLATTICES FROM X-RAY-DIFFRACTION [J].
FULLERTON, EE ;
SCHULLER, IK ;
VANDERSTRAETEN, H ;
BRUYNSERAEDE, Y .
PHYSICAL REVIEW B, 1992, 45 (16) :9292-9310
[4]   STUDYING THE INTERFACE OF AU-CU SUPERLATTICES [J].
GLADYSZEWSKI, G .
THIN SOLID FILMS, 1989, 170 (01) :99-106
[5]  
Guinier A, 1963, X-ray Diffraction
[6]   X-ray interference in partially ordered layer lattices [J].
Hendricks, S ;
Teller, E .
JOURNAL OF CHEMICAL PHYSICS, 1942, 10 (03) :147-167
[7]  
KRZANOWSKI JE, 1992, MATER RES SOC SYMP P, V239, P509
[8]   Stabilization of cubic AlN in epitaxial AlN/TiN superlattices [J].
Madan, A ;
Kim, IW ;
Cheng, SC ;
Yashar, P ;
Dravid, VP ;
Barnett, SA .
PHYSICAL REVIEW LETTERS, 1997, 78 (09) :1743-1746
[9]   Growth and characterization of epitaxial Mo/NbN superlattices [J].
Madan, A ;
Chu, X ;
Barnett, SA .
APPLIED PHYSICS LETTERS, 1996, 68 (16) :2198-2200
[10]  
MADAN A, UNPUB