Tuning the size of silver deposits by templated electrodeposition using agarose gels

被引:13
作者
Hasse, U [1 ]
Scholz, F [1 ]
机构
[1] Univ Greifswald, Inst Chem, D-17489 Greifswald, Germany
关键词
atomic force microscopy; electrochemistry; silver deposition; templates;
D O I
10.1007/s10008-005-0694-2
中图分类号
O646 [电化学、电解、磁化学];
学科分类号
081704 ;
摘要
Tuning the size of electrochemically deposited silver crystals is possible by using template layers of agarose gels of certain concentrations on platinum electrodes. The size of the silver crystals can be controlled in the range of 100 to 400 nm by choosing the appropriate agarose concentration. The obtained crystal sizes match very well with the size of the pores that have been reported in literature for the used agarose concentrations. This is also a good proof of the correctness of the earlier pore-size estimations applying other techniques.
引用
收藏
页码:380 / 382
页数:3
相关论文
共 15 条
[1]   TRANSPORT PHENOMENA AND GROWTH MODES OF SILVER ELECTRODEPOSITS [J].
CARRO, P ;
AMBROSOLIO, S ;
MARCHIANO, SL ;
CREUS, AH ;
SALVAREZZA, RC ;
ARVIA, AJ .
JOURNAL OF ELECTROANALYTICAL CHEMISTRY, 1995, 396 (1-2) :183-195
[2]  
DERIU A, 1991, PROG COLL POL SCI S, V84, P461
[3]   In situ AFM observation of the electrochemical reduction of a single silver sulphide crystal and the recrystallization of the resulting silver crystal [J].
Hasse, U ;
Scholz, F .
ELECTROCHEMISTRY COMMUNICATIONS, 2005, 7 (02) :173-176
[4]   Nucleation at three-phase junction lines: in situ atomic force microscopy of the electrochemical reduction of sub-micrometer size silver and mercury(I) halide crystals immobilized on solid electrodes [J].
Hasse, U ;
Wagner, K ;
Scholz, F .
JOURNAL OF SOLID STATE ELECTROCHEMISTRY, 2004, 8 (10) :842-853
[5]   In situ AFM evidence of the involvement of an oversaturated solution in the course of oxidation of silver nanocrystals to silver iodide and bromide crystals [J].
Hasse, U ;
Scholz, F .
ELECTROCHEMISTRY COMMUNICATIONS, 2004, 6 (04) :409-412
[6]   In situ atomic force microscopy of the reduction of lead oxide nanocrystals immobilised on an electrode surface [J].
Hasse, U ;
Scholz, F .
ELECTROCHEMISTRY COMMUNICATIONS, 2001, 3 (08) :429-434
[7]  
HASSE U, 2003, J ELECTROANAL CHEM, V13, P556
[8]  
LOTTSPEICH F, 1998, BIOANALYTIK, P225
[9]   Agarose gel structure using atomic force microscopy: Gel concentration and ionic strength effects [J].
Maaloum, M ;
Pernodet, N ;
Tinland, B .
ELECTROPHORESIS, 1998, 19 (10) :1606-1610
[10]  
Martin CR, 1999, ELECTROANAL CHEM, V21, P1