Low temperature synthesis of hexagonal phase ZnS nanocrystals by thermolysis of an air-stable single-source molecular precursor in air

被引：59

作者：

Liu, W ^{[1
]}

机构：

[1] Yangzhou Univ, Coll Chem & Chem Engn, Yangzhou 225002, Peoples R China

来源：

MATERIALS LETTERS | 2006年 / 60卷 / 04期

关键词：

low temperature synthesis; single-source molecular precursor; nanomaterials; zinc sulfide; semiconducting II-VI materials;

D O I：

10.1016/j.matlet.2005.09.033

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

Pure metastable hexagonal phase ZnS nanocrystals with the sizes in the range of 2.8 to 6.6 nm were synthesized by thermolysis of an air-stable, easily obtained single-source molecular precursor (zinc diethyldithiocarbamate, Zn-(DDTC)(2)) in air at 280 degrees C for 12 h, and characterized by means of powder X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), transmission electron microscopy (TEM) and selected-area electron diffraction (SAED), and UV-Vis absorption spectrum. (c) 2005 Elsevier B.V. All rights reserved.

引用

页码：551 / 554

页数：4

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