Synthesis of dicobalt hexacarbonyl 5-p-tolylethynyl-2′-deoxyuridine

被引：25

作者：

Esho, N

Davies, B

Lee, J

Dembinski, R

机构：

[1] Oakland Univ, Dept Chem, Rochester, MI 48309 USA

[2] Oakland Univ, Biomed Res Ctr, Rochester, MI 48309 USA

来源：

CHEMICAL COMMUNICATIONS | 2002年 / 04期

关键词：

D O I：

10.1039/b109501c

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Reactions of 5-p-tolylethynyl-2'-deoxyuridine and 3',5'-di-O-acetyl-5-p-tolylethynyl-2'-deoxyuridine with Co-2(CO)(8) in THF gave 5-p-tolC(2)[Co-2(CO)(6)]-2'-deoxyuridine and 3',5'-di-O-acetyl-5-p-tolC(2)[Co-2(CO)(6)]-2'-deoxyuridine (92 and 66%).

引用

页码：332 / 333

页数：2

共 33 条

[1] Synthesis of the first ferrocene-labeled dideoxynucleotide and its use for 3′-redox end-labeling of 5′-modified single-stranded oligonucleotides [J].

Anne, A ;

Blanc, B ;

Moiroux, J .

BIOCONJUGATE CHEMISTRY, 2001, 12 (03) :396-405

[2] Quantitative analysis of receptors for adenosine nucleotides obtained via in vitro selection from a library incorporating a cationic nucleotide analog [J].

Battersby, TR ;

Ang, DN ;

Burgstaller, P ;

Jurczyk, SC ;

Bowser, MT ;

Buchanan, DD ;

Kennedy, RT ;

Benner, SA .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1999, 121 (42) :9781-9789

[3] On-column derivatization of oligodeoxynucleotides with ferrocene [J].

Beilstein, AE ;

Grinstaff, MW .

CHEMICAL COMMUNICATIONS, 2000, (06) :509-510

[4] Influence of intervening mismatches on long-range guanine oxidation in DNA duplexes [J].

Bhattacharya, PK ;

Barton, JK .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2001, 123 (36) :8649-8656

[5] Bicyclic nucleoside inhibitors of varicella-zoster virus (VZV): The effect of a terminal halogen substitution in the side-chain [J].

Brancale, A ;

McGuigan, C ;

Andrei, G ;

Snoeck, R ;

De Clercq, E ;

Balzarini, J .

BIOORGANIC & MEDICINAL CHEMISTRY LETTERS, 2000, 10 (11) :1215-1217

[6] Synthesis of a modified thymidine monomer for site-specific incorporation of reporter groups into oligonucleotides [J].

Brown, LJ ;

May, JP ;

Brown, T .

TETRAHEDRON LETTERS, 2001, 42 (13) :2587-2591

[7] Recent advances in the Pauson-Khand reaction and related [2+2+1] cycloadditions [J].

Brummond, KM ;

Kent, JL .

TETRAHEDRON, 2000, 56 (21) :3263-3283

[8]

Cammenga H. K., 1995, Angew. Chem, V107, P1284

[9]

Chung YK, 1999, COORDIN CHEM REV, V188, P297

[10] ON THE REACTIVITY OF ACETYLENES COORDINATED TO COBALT .9. EFFECTS OF SUBSTITUTION AND COORDINATION ON THE C-13-NMR CHEMICAL-SHIFTS OF THE SP CARBONS OF (MU(2)-R(1)C(2)R(2))CO-2(CO)(6) COMPLEXES - MOLECULAR-STRUCTURE OF (MU(2)-PHC(2)SIPH(3))CO-2(CO)(6) [J].

HAPP, B ;

BARTIK, T ;

ZUCCHI, C ;

ROSSI, MC ;

GHELFI, F ;

PALYI, G ;

VARADI, G ;

SZALONTAI, G ;

HORVATH, IT ;

CHIESIVILLA, A ;

GUASTINI, C .

ORGANOMETALLICS, 1995, 14 (02) :809-819

← 1 2 3 4 →