Electrolytic partial fluorination of organic compounds.: Part 56:: Highly regioselective anodic mono- and difluorination of s-triazolo[3,4-b][1,3,4]thiadiazine derivatives

被引:28
作者
Shaaban, MR [1 ]
Fuchigami, T [1 ]
机构
[1] Tokyo Inst Technol, Dept Elect Chem, Midori Ku, Yokohama, Kanagawa 2268502, Japan
关键词
D O I
10.1016/S0040-4039(01)02133-5
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
Constant potential anodic oxidation of s-triazolo[3,4-h][1.3,4]thiadiazine derivatives in DME containing Et(4)NF(.)4HF using an undivided cell provided the corresponding 7-monofluorinated products predominantly in good to moderate yields. 7,7-Difluorination. was also anodically achieved. (C) 2002 Elsevier Science Ltd. All rights reserved.
引用
收藏
页码:273 / 276
页数:4
相关论文
共 30 条