Convenient solvothermal synthesis and phase control of nickel selenides with different morphologies

被引：44

作者：

Han, ZH ^{[1
]}

Yu, SH

Li, YP

Zhao, HG

Li, FQ

Xie, Y

Qian, YT

机构：

[1] Univ Sci & Technol China, Dept Chem, Hefei 230026, Anhui, Peoples R China

[2] Univ Sci & Technol China, Struct Res Lab, Hefei 230026, Anhui, Peoples R China

来源：

CHEMISTRY OF MATERIALS | 1999年 / 11卷 / 09期

关键词：

D O I：

10.1021/cm990198q

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

A series of well-crystallized nickel selenides, including NiSe2, Ni0.85Se, and Ni3Se2 have been synthesized via a solvothermal technique. The single phases can be conveniently obtained under controlled conditions. Interestingly, the crystals of single phases as well as the mixtures obtained in selected solvents own different morphologies. The solution synthetic route introduced in this paper may be applicable to a broad range of transition metal chalcogenides with different morphologies.

引用

页码：2302 / +

页数：4

共 20 条

[1] RAPID SOLID-STATE SYNTHESIS OF MATERIALS FROM MOLYBDENUM-DISULFIDE TO REFRACTORIES [J].

BONNEAU, PR ;

JARVIS, RF ;

KANER, RB .

NATURE, 1991, 349 (6309) :510-512

[2] NI23SE12(PET3)13 - AN INTRAMOLECULAR INTERGROWTH OF NISE AND NI [J].

BRENNAN, JG ;

SIEGRIST, T ;

KWON, YU ;

STUCZYNSKI, SM ;

STEIGERWALD, ML .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1992, 114 (26) :10334-10338

[3] ELECTRONIC-STRUCTURE OF SOME 3D TRANSITION-METAL PYRITES [J].

FOLKERTS, W ;

SAWATZKY, GA ;

HAAS, C ;

DEGROOT, RA ;

HILLEBRECHT, FU .

JOURNAL OF PHYSICS C-SOLID STATE PHYSICS, 1987, 20 (26) :4135-4144

[4] BLUE-GREEN LASER-DIODES [J].

HAASE, MA ;

QIU, J ;

DEPUYDT, JM ;

CHENG, H .

APPLIED PHYSICS LETTERS, 1991, 59 (11) :1272-1274

[5]

HENSHAW S, 1997, J CHEM SOC DA, P231

[6]

HIROTO U, Patent No. 01298010

[7]

HULLIGER J, 1994, ANGEW CHEM INT EDIT, V33, P143, DOI 10.1002/anie.199401431

[8]

KITAHARA K, Patent No. 03178312

[9]

MAHADEV KN, Patent No. 5030437

[10]

MASAAKI I, 1987, XRAY SPECTROM, V16, P73

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