Solvothermal route to Bi3Se4 nanorods at low temperature

被引：13

作者：

Liu, YF

Zeng, JH

Zhang, WX

Yu, WC

Qian, YT ^{[1
]}

Cao, JB

Zhang, WQ

机构：

[1] Univ Sci & Technol China, Struct Res Lab, Hefei 230026, Anhui, Peoples R China

[2] Univ Sci & Technol China, Dept Chem, Hefei 230026, Anhui, Peoples R China

来源：

JOURNAL OF MATERIALS RESEARCH | 2001年 / 16卷 / 12期

关键词：

D O I：

10.1557/JMR.2001.0464

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

Nanorods Bi3Se4 were synthesized directly through the reaction between BiCl3 and elemental selenium in an autoclave with hydrazine hydrate as solvent at 165 degreesC for 10 h. X-ray powder diffraction patterns, x-ray photoelectron spectra, and transmission electron microscope images show that the products are well-crystallized hexagonal Bi3Se4 nanorods. The solvent hydrazine hydrate played an important role in formation and growth of Bi3Se4 nanorods. The possible reaction mechanism was proposed.

引用

页码：3361 / 3365

页数：5

共 36 条

[1] CARBON NANOTUBES AS REMOVABLE TEMPLATES FOR METAL-OXIDE NANOCOMPOSITES AND NANOSTRUCTURES [J].