Modern applications of a new 300 kV field emission transmission electron microscope to the study of advanced materials

被引:4
作者
Bando, Y
Kurashima, K
Nakano, S
机构
[1] Natl. Inst. for Res. in Inorg. Mat., Tsukuba, Ibaraki 305
关键词
D O I
10.1016/0955-2219(95)00087-9
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
Some instrumental features of a new 300 kV analytical transmission electron microscope with a field emission gun and its applications to structure and composition analysis of advanced materials at nanometer scales are given. In the few microscope, a fine electron probe of about 0.5 nm in size with a probe current of about 0.1 nA can be routinely applied for elemental analysis in combination with high resolution lattice imaging. A crystal structure of 33R-AlN polytype is determined from the single atomic layer level analysis using energy dispersive X-ray spectrometry (EDS). It is also shown that a Mew cubic B-C-N compound is identified to be a diamond-like structure from the observation of lattice image and electron energy loss spectrometry (EELS).
引用
收藏
页码:379 / 384
页数:6
相关论文
共 15 条
[1]  
BANDO Y, 1989, J ELECTRON MICROSC, V38, pS81
[2]   ANALYTICAL TRANSMISSION ELECTRON-MICROSCOPY IN MATERIALS SCIENCE [J].
BANDO, Y .
MATERIALS TRANSACTIONS JIM, 1990, 31 (07) :538-544
[3]  
BANDO Y, 1994, MATER RES SOC SYMP P, V346, P733, DOI 10.1557/PROC-346-733
[4]   STRUCTURE AND COMPOSITION ANALYSIS OF SILICON ALUMINUM OXYNITRIDE POLYTYPES BY COMBINED USE OF STRUCTURE IMAGING AND MICROANALYSIS [J].
BANDO, Y ;
MITOMO, M ;
KITAMI, Y ;
IZUMI, F .
JOURNAL OF MICROSCOPY, 1986, 142 :235-246
[5]   A NEWLY DEVELOPED 300 KV FIELD-EMISSION ANALYTICAL TRANSMISSION ELECTRON-MICROSCOPE [J].
BANDO, Y ;
KITAMI, Y ;
TOMITA, T ;
HONDA, T ;
ISHIDA, Y .
JAPANESE JOURNAL OF APPLIED PHYSICS PART 2-LETTERS & EXPRESS LETTERS, 1993, 32 (11B) :L1704-L1706
[6]  
BANDO Y, 1994, P 13 INT C EL MICR, P591
[7]  
BANDO Y, 1994, MICROBEAM ANAL, V3, P276
[8]   AL10N8O3 AND AL9N7O3, 2 NEW REPEATED-LAYER STRUCTURES IN THE AIN-AL2O3 SYSTEM [J].
BARTRAM, SF ;
SLACK, GA .
ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE, 1979, 35 (SEP) :2281-2283
[9]  
COENE W, 1992, P 50 ANN M EL MICR A, P100
[10]  
ISAKOZAWA S, 1989, P 47 ANN M EL MICR S, P112