Silver nanoparticles growth in a mesoporous silica film templated with the F127 triblock copolymer

被引:23
作者
Bois, L. [1 ]
Bessueille, F. [2 ]
Chassagneux, F. [1 ]
Battie, Y. [3 ]
Destouches, N. [3 ]
Hubert, C. [3 ]
Boukenter, A. [3 ]
Parola, S. [1 ]
机构
[1] Univ Lyon 1, CNRS, Lab Multimat & Interfaces, UMR 5615, F-69622 Villeurbanne, France
[2] Univ Lyon 1, CNRS, Sci Analyt Lab, UMR 5180, F-69622 Villeurbanne, France
[3] Univ St Etienne, CNRS, Lab Hubert Curien, UMR 5516,LTSI, F-42000 St Etienne, France
关键词
thin films; sol-gel growth; electron microscopy; optical properties;
D O I
10.1016/j.colsurfa.2008.04.045
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
The elaboration of mesoporous silica films supporting silver nanoparticles is described. Mesoporous silica films were infiltrated with silver salt solutions of different concentrations and chemical reduction treatment was performed in situ by NaBH4. The films have been characterized by TEM, AFM, XRD, and UV-vis spectroscopy. Homogeneous distributions of silver nanoparticles have been obtained by this method. (C) 2008 Elsevier B.V. All rights reserved.
引用
收藏
页码:86 / 92
页数:7
相关论文
共 62 条
[1]   Synthesis of silver nanowires inside mesoporous MCM-41 host [J].
Adhyapak, PV ;
Karandikar, P ;
Vijayamohanan, K ;
Athawale, AA ;
Chandwadkar, AJ .
MATERIALS LETTERS, 2004, 58 (7-8) :1168-1171
[2]   Silver nanoparticle growth in 3D-hexagonal mesoporous silica films [J].
Besson, S ;
Gacoin, T ;
Ricolleau, C ;
Boilot, JP .
CHEMICAL COMMUNICATIONS, 2003, (03) :360-361
[3]  
Besson S, 2002, MATER RES SOC SYMP P, V707, P119
[4]   Optical study of redox process of Ag nanoparticles at high temperature [J].
Bi, Huijuan ;
Cai, Weiping ;
Kan, Caixia ;
Zhang, Lide ;
Martin, D. ;
Träger, F. .
Journal of Applied Physics, 2002, 92 (12) :7491-7497
[5]   Optical absorption of Ag oligomers dispersed within pores of mesoporous silica [J].
Bi, HJ ;
Cai, WP ;
Shi, HZ ;
Liu, X .
CHEMICAL PHYSICS LETTERS, 2002, 357 (3-4) :249-254
[6]  
Bjerneld EJ, 2002, CHEMPHYSCHEM, V3, P116, DOI 10.1002/1439-7641(20020118)3:1<116::AID-CPHC116>3.0.CO
[7]  
2-2
[8]   Porosity and mechanical properties of mesoporous thin films assessed by environmental ellipsometric porosimetry [J].
Boissiere, C ;
Grosso, D ;
Lepoutre, S ;
Nicole, L ;
Bruneau, AB ;
Sanchez, C .
LANGMUIR, 2005, 21 (26) :12362-12371
[9]   Some recent advances in nanostructure preparation from gold and silver particles: a short topical review [J].
Brust, M ;
Kiely, CJ .
COLLOIDS AND SURFACES A-PHYSICOCHEMICAL AND ENGINEERING ASPECTS, 2002, 202 (2-3) :175-186
[10]  
Cai WP, 1997, J PHYS-CONDENS MAT, V9, P7257, DOI 10.1088/0953-8984/9/34/015