Purification of single-wall carbon nanotubes

被引：235

作者：

Shi, ZJ ^{[1
]}

Lian, YF ^{[1
]}

Liao, FH ^{[1
]}

Zhou, XH ^{[1
]}

Gu, ZN ^{[1
]}

Zhang, YG ^{[1
]}

Iijima, S ^{[1
]}

机构：

[1] Peking Univ, Dept Chem, Beijing 100871, Peoples R China

来源：

SOLID STATE COMMUNICATIONS | 1999年 / 112卷 / 01期

基金：

中国国家自然科学基金;

关键词：

fullerenes; chemical synthesis; scanning and transmission electron microscopy;

D O I：

10.1016/S0038-1098(99)00278-1

中图分类号：

O469 [凝聚态物理学];

学科分类号：

070205 ;

摘要：

With Y-Ni alloy and CaC2-Ni as catalyst, large-scale single-wall carbon nanotubes (SWCNTs) were produced by d.c. arc-discharge method. The yield of SWCNTs and the composition of the raw-soot was quantified with thermogravimetric analysis (TGA). The burning temperature of SWCNTs in air was also determined. On these bases, 350 degrees C was chosen for the first step purification of SWCNTs. Combining with the micro-filtration method, larger than 90% purity of SWCNTs and high purity of carbon nanoparticles were obtained. (C) 1999 Elsevier Science Ltd. All rights reserved.

引用

页码：35 / 37

页数：3

共 10 条

[1] Large-scale production of single-walled carbon nanotubes by the electric-arc technique
Journet, C
Maser, WK
Bernier, P
Loiseau, A
delaChapelle, ML
Lefrant, S
Deniard, P
Lee, R
Fischer, JE
[J]. NATURE, 1997, 388 (6644) : 756 - 758
[2] THERMOGRAVIMETRIC ANALYSIS OF CARBON NANOTUBES AND NANOPARTICLES
PANG, LSK
SAXBY, JD
CHATFIELD, SP
[J]. JOURNAL OF PHYSICAL CHEMISTRY, 1993, 97 (27) : 6941 - 6942
[3] Large-scale purification of single-wall carbon nanotubes: process, product, and characterization
Rinzler, AG
Liu, J
Dai, H
Nikolaev, P
Huffman, CB
Rodriguez-Macias, FJ
Boul, PJ
Lu, AH
Heymann, D
Colbert, DT
Lee, RS
Fischer, JE
Rao, AM
Eklund, PC
Smalley, RE
[J]. APPLIED PHYSICS A-MATERIALS SCIENCE & PROCESSING, 1998, 67 (01): : 29 - 37
[4] High yield of single-wall carbon nanotubes by arc discharge using Rh-Pt mixed catalysts
Saito, Y
Tani, Y
Miyagawa, N
Mitsushima, K
Kasuya, A
Nishina, Y
[J]. CHEMICAL PHYSICS LETTERS, 1998, 294 (06) : 593 - 598
[5] Superstrong nanotubes show they are smart, too
Service, RF
[J]. SCIENCE, 1998, 281 (5379) : 940 - 942
[6] Mass-production of single-wall carbon nanotubes by arc discharge method
Shi, ZJ
Lian, YF
Zhou, XH
Gu, ZN
Zhang, YG
Iijima, S
Zhou, LX
Yue, KT
Zhang, SL
[J]. CARBON, 1999, 37 (09) : 1449 - 1453
[7] TAKAHASHI H, 1996, J MAT SCI ENG A, V217, P42
[8] Crystalline ropes of metallic carbon nanotubes
Thess, A
Lee, R
Nikolaev, P
Dai, HJ
Petit, P
Robert, J
Xu, CH
Lee, YH
Kim, SG
Rinzler, AG
Colbert, DT
Scuseria, GE
Tomanek, D
Fischer, JE
Smalley, RE
[J]. SCIENCE, 1996, 273 (5274) : 483 - 487
[9] Purifying single-walled nanotubes
Tohji, K
Goto, T
Takahashi, H
Shinoda, Y
Shimizu, N
Jeyadevan, B
Matsuoka, I
Saito, Y
Kasuya, A
Ohsuna, T
Hiraga, H
Nishina, Y
[J]. NATURE, 1996, 383 (6602) : 679 - 679
[10] Defects in arc-discharge-produced single-walled carbon nanotubes
Zhang, Y
Iijima, S
Shi, Z
Gu, Z
[J]. PHILOSOPHICAL MAGAZINE LETTERS, 1999, 79 (07) : 473 - 479

← 1 →