Determination of chlorinated pesticides in water by SPME/GC

被引:49
作者
Boussahel, R
Bouland, S
Moussaoui, KM
Baudu, M
Montiel, A
机构
[1] SAGEP, F-75014 Paris, France
[2] Ecole Natl Polytech, El Harrach 16200, Algeria
[3] Fac Sci Limoges, Lab Sci Eau & Environm, F-87060 Limoges, France
关键词
chlorinated pesticides; SPME; water analysis; microextraction;
D O I
10.1016/S0043-1354(01)00372-4
中图分类号
X [环境科学、安全科学];
学科分类号
08 ; 0830 ;
摘要
Solid-phase microextraction (SPME) followed by gas chromatography (GC) coupled with an electron capture detector has been applied for the analysis of chlorinated pesticides in water. Molecule adsorption on 100 mum polydimethylsiloxane (PDMS) fibers was activated by immersion of the whole fiber-sample system in an ultrasonic bath. The good reproducibility, low detection limits and wide linear ranges obtained encourage the use of this technique in water control. (C) 2002 Published by Elsevier Science Ltd.
引用
收藏
页码:1909 / 1911
页数:3
相关论文
共 11 条
[1]  
ARTHUR CL, 1992, LC GC-MAG SEP SCI, V10, P656
[2]  
BELARDI RP, 1989, WATER POLLUTION RES, V24, P37
[3]   Inter-laboratory validation of solid-phase microextraction for the determination of triazine herbicides and their degradation products at ng/1 level in water samples [J].
Ferrari, R ;
Nilsson, T ;
Arena, R ;
Arlati, P ;
Bartolucci, C ;
Basla, R ;
Cioni, F ;
Del Carlo, G ;
Dellavedova, P ;
Fattore, E ;
Fungi, M ;
Grote, C ;
Guidotti, M ;
Morgillo, S ;
Müller, L ;
Volante, M .
JOURNAL OF CHROMATOGRAPHY A, 1998, 795 (02) :371-376
[4]   Solid-phase microextraction with rotation of the microfiber [J].
Geppert, H .
ANALYTICAL CHEMISTRY, 1998, 70 (18) :3981-3982
[5]   Theory of analyte extraction by selected porous polymer SPME fibres [J].
Górecki, T ;
Yu, XM ;
Pawliszyn, J .
ANALYST, 1999, 124 (05) :643-649
[6]   Use of solid phase microextraction for the quantitative determination of herbicides in soil and water samples [J].
Hernandez, F ;
Beltran, J ;
Lopez, FJ ;
Gaspar, JV .
ANALYTICAL CHEMISTRY, 2000, 72 (10) :2313-2322
[7]  
Massat F., 1999, SPECTRA ANAL, V208, P23
[8]  
Pawliszyn J., 1997, SOLID PHASE MICROEXT
[9]   Solid-phase microextraction method for the quantitative analysis of styrene in water [J].
Silva, FC ;
de Carvalho, CR ;
Cardeal, ZD .
JOURNAL OF CHROMATOGRAPHIC SCIENCE, 2000, 38 (07) :315-318
[10]   Solid-phase microextraction for the analysis of biological samples [J].
Theodoridis, G ;
Koster, EHM ;
de Jong, GJ .
JOURNAL OF CHROMATOGRAPHY B-ANALYTICAL TECHNOLOGIES IN THE BIOMEDICAL AND LIFE SCIENCES, 2000, 745 (01) :49-82