Green synthesis of ZnO nanoparticles in a room-temperature ionic liquid 1-ethyl-3-methylimidazolium bis(trifluoromethylsulfonyl)imide

被引:48
作者
Goharshadi, Elaheh K. [1 ]
Ding, Yulong [2 ]
Nancarrow, Paul [3 ,4 ]
机构
[1] Ferdowsi Univ Mashhad, Dept Chem, Mashhad 91779, Iran
[2] Univ Leeds, Inst Particle Sci & Engn, Leeds, W Yorkshire, England
[3] Queens Univ, Sch Chem & Chem Engn, Belfast, Antrim, North Ireland
[4] Queens Univ, QUILL Res Ctr, Belfast, Antrim, North Ireland
基金
英国工程与自然科学研究理事会;
关键词
nanostructures; semiconductors; chemical synthesis; X-ray diffraction;
D O I
10.1016/j.jpcs.2008.03.002
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Nanoparticles of ZnO with the wurtzite structure have been successfully synthesized via a microwave through the decomposition of zinc acetate dihydrate in an ionic liquid, 1-ethyl-3-methylimidazolium bis(trifluoromethylsulfonyl)imide, as a solvent. Fundamental characterizations including X-ray diffraction (XRD), scanning electron microscopy (SEM), and transmission electron microscopy (TEM) were conducted for the ZnO nanostructures. To explore the growth mechanism, the samples have been prepared in different irradiation time and also cetyltrimethylammonium bromide (CTAB) has been used as the capping reagent. (c) 2008 Elsevier Ltd. All rights reserved.
引用
收藏
页码:2057 / 2060
页数:4
相关论文
共 26 条
[21]   Synthesis of CoPt nanorods in ionic liquids [J].
Wang, Y ;
Yang, H .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2005, 127 (15) :5316-5317
[22]   Oleic acid as the capping agent in the synthesis of noble metal nanoparticles in imidazolium-based ionic liquids [J].
Wang, Yong ;
Yang, Hong .
CHEMICAL COMMUNICATIONS, 2006, (24) :2545-2547
[23]  
Wasserscheid P., 2000, ANGEW CHEM INT EDIT, V112, P3926, DOI DOI 10.1002/1521-3773(20001103)39:21<3772::AID-ANIE3772>3.0.CO
[24]  
2-5
[25]   Room-temperature ionic liquids. Solvents for synthesis and catalysis [J].
Welton, T .
CHEMICAL REVIEWS, 1999, 99 (08) :2071-2083
[26]   Ionic liquids: Ion mobilities, glass temperatures, and fragilities [J].
Xu, W ;
Cooper, EI ;
Angell, CA .
JOURNAL OF PHYSICAL CHEMISTRY B, 2003, 107 (25) :6170-6178