Spatial Resolution in Atom Probe Tomography

被引:163
作者
Gault, Baptiste [1 ,2 ]
Moody, Michael P. [1 ]
De Geuser, Frederic [3 ]
La Fontaine, Alex [1 ]
Stephenson, Leigh T. [1 ]
Haley, Daniel [1 ]
Ringer, Simon P. [1 ]
机构
[1] Univ Sydney, Australian Key Ctr Microscopy & Microanal, Sydney, NSW 2006, Australia
[2] Univ Oxford, Dept Mat, Oxford OX1 3PH, England
[3] UJF, Grenoble INP, CNRS, SIMaP UMR 5266, St Martin Dheres, France
基金
澳大利亚研究理事会;
关键词
atom probe tomography; resolution; tomographic reconstruction; spatial distribution maps; trajectory aberration; FIELD EVAPORATION; LOCAL MAGNIFICATION; FOURIER-TRANSFORM; POST-IONIZATION; RECONSTRUCTION; INSTRUMENT; MICROSCOPY; SURFACES; IONS;
D O I
10.1017/S1431927609991267
中图分类号
T [工业技术];
学科分类号
120111 [工业工程];
摘要
This article addresses gaps in definitions and a lack of standard measurement techniques to assess the spatial resolution in atom probe tomography. This resolution is known to be anisotropic, being better in-depth than laterally. Generally the presence of atomic planes in the tomographic reconstruction is considered as being a Sufficient proof of the quality of the spatial resolution of the instrument. Based oil advanced spatial distribution maps, an analysis methodology that interrogates the local neighborhood of the atoms within the tomographic reconstruction, it is shown how both the in-depth and the lateral resolution can be quantified. The influences of the crystallography and the temperature are investigated, and models are proposed to explain the observed results. We demonstrate that the absolute value of resolution is specimen specific.
引用
收藏
页码:99 / 110
页数:12
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