The tetrameric macrocycle [{P(μ-N-tBu)}2NH]4

被引:64
作者
Bashall, A
Doyle, EL
Tubb, C
Kidd, SJ
McPartlin, M
Woods, AD
Wright, DS
机构
[1] Univ Cambridge, Dept Chem, Cambridge CB2 1EW, England
[2] Univ N London, Sch Chem, London N7 8DB, England
关键词
D O I
10.1039/b107650g
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
The 1:1 reaction of the symmetrical dimers [ClP(mu -(NBu)-Bu-t)](2) 1 and [H2NP(mu -(NBu)-Bu-t)](2) 2 in thf-Et3N gives the tetrameric macrocycle [{P(mu -(NBu)-Bu-t)}(2)NH](4) 3 (67%); consisting of four P-2(mu -(NBu)-Bu-t)(2) rings linked by endo N-H groups.
引用
收藏
页码:2542 / 2543
页数:2
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