Synthesis of deuterium labelled desulfoglucosinolates as internal standards for LC-MS analysis

被引：19

作者：

Robertson, AAB ^{[1
]}

Botting, NP ^{[1
]}

机构：

[1] Univ St Andrews, Sch Chem, St Andrews KY16 9ST, Fife, Scotland

来源：

TETRAHEDRON | 1999年 / 55卷 / 46期

关键词：

thioglycosides; labelling; plants; insects;

D O I：

10.1016/S0040-4020(99)00817-0

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

The syntheses of three deuterium labelled desulfoglucosinolates are described. These are the phenethyl, 1-methoxyindolyl and 4-methoxyindolyl derivatives. The compounds were prepared as internal standards for use in the quantitative LC-MS analysis of glucosinolates to improve the sensitivity of the analytical procedure. (C) 1999 Elsevier Science Ltd. All rights reserved.

引用

页码：13269 / 13284

页数：16

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