Solvothermal synthesis of CdS nanowires using L-cysteine as sulfur source and their characterization

被引:39
作者
Gai, Hongde [1 ]
Wu, Youshi [1 ]
Wu, Lili [1 ]
Wang, Zhigang [2 ]
Shi, Yuanchang [1 ]
Jing, Min [1 ]
Zou, Ke [1 ]
机构
[1] Shandong Univ, Coll Mat Sci & Engn, Jinan 250061, Peoples R China
[2] Shandong Jianzhu Univ, Coll Mat Sci & Engn, Jinan 250101, Peoples R China
来源
APPLIED PHYSICS A-MATERIALS SCIENCE & PROCESSING | 2008年 / 91卷 / 01期
关键词
D O I
10.1007/s00339-007-4359-0
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
An effective solvothermal reaction route has been developed for large-scale synthesis of CdS nanowires. L-cysteine was used as both sulfur source and capping reagent. The nanowires obtained were characterized by XRD, SEM, TEM, HRTEM, UV-Vis and PL. On the basis of time-resolved experiments, a possible growth mechanism was proposed. FTIR analysis confirmed the formation of Cd-cysteine complex and peptide during the reaction. The mechanism was further supported by comparative experiments with other sulfur sources.
引用
收藏
页码:69 / 72
页数:4
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