Solvent-free phase transfer catalysis under microwaves in fullerene chemistry. A convenient preparation of N-alkylpyrrolidino[60]fullerenes.

被引：48

作者：

de la Cruz, P

de la Hoz, A

Font, LM

Langa, F ^{[1
]}

Perez-Rodriguez, MC

机构：

[1] Univ Castilla La Mancha, Fac Quim, Dept Quim Organ, E-45001 Toledo, Spain

[2] Janssen Cilag SA, Ctr Invest, Toledo 45009, Spain

来源：

TETRAHEDRON LETTERS | 1998年 / 39卷 / 33期

关键词：

D O I：

10.1016/S0040-4039(98)01245-3

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

A facile synthesis of a series of N-alkylpyrrolidino[60]fullerenes by phase transfer catalysis without solvent under microwave irradiation is described. (C) 1998 Elsevier Science Ltd. All rights reserved.

引用

页码：6053 / 6056

页数：4

共 29 条

[1] ABENHAIM D, 1994, HETEROCYCLES, V38, P793
[2] Solvent-free benzylations of 2-pyridone. Regiospecific N- or C-alkylation
Almena, I
DiazOrtiz, A
DiezBarra, E
delaHoz, A
Loupy, A
[J]. CHEMISTRY LETTERS, 1996, (05) : 333 - 334
[3] Bogdal D, 1996, SYNLETT, P873
[4] BRAM G, 1989, B SOC CHIM FR, P247
[5] BRAM G, 1985, ISRAEL J CHEM, V26, P291
[6] BRAM G, 1992, MICROWAVE ACTIVATION
[7] Silica gel catalysed Knoevenagel condensation in Dry Media under microwave irradiation
delaCruz, P
DiezBarra, E
Loupy, A
Langa, F
[J]. TETRAHEDRON LETTERS, 1996, 37 (07) : 1113 - 1116
[8] Cycloadditions to [60]fullerene using microwave irradiation: A convenient and expeditious procedure.
delaCruz, P
delaHoz, A
Langa, F
Illescas, B
Martin, N
[J]. TETRAHEDRON, 1997, 53 (07) : 2599 - 2608
[9] DOU HJM, 1976, B SOC CHIM FR, P1981
[10] HIRSCH A, 1995, SYNTHESIS-STUTTGART, P895

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