Carbon-encapsulated magnetic nanoparticles spontaneously formed by thermolysis route

被引：8

作者：

Bystrzejewski, M. ^{[1
]}

Huczko, A. ^{[1
]}

Lange, H. ^{[1
]}

Baranowski, P. ^{[1
]}

Kaszuwara, W. ^{[2
]}

Cudzilo, S. ^{[3
]}

Kowalska, E. ^{[4
]}

Rummeli, M. H. ^{[5
]}

Gemming, T. ^{[5
]}

机构：

[1] Warsaw Univ, Dept Chem, PL-02093 Warsaw, Poland

[2] Warsaw Univ Technol, Fac Mat Sci & Engn, Warsaw, Poland

[3] Mil Univ Technol WAT, Warsaw, Poland

[4] Tele & Radio Res Inst, Warsaw, Poland

[5] IFW Dresden, Dresden, Germany

来源：

FULLERENES NANOTUBES AND CARBON NANOSTRUCTURES | 2008年 / 16卷 / 04期

关键词：

carbon nanostructures; thermolysis; magnetic nanoparticles; X-ray; diffraction; Raman spectroscopy;

D O I：

10.1080/15363830802171503

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 [物理化学]; 081704 [应用化学];

摘要：

A new method for producing carbon-encapsulated magnetic nanoparticles using a thermolysis route is developed. The method is based on dechlorination of C6Cl6 with NaN3 in the presence of Fe or Fe14Nd2B magnetic alloy. The as-obtained products contained carbon-encapsulated magnetic nanoparticles with the diameters between 20 and 60nm. The products were purified and their composition and morphology were studied by means of SEM, TEM, XRD and TG-DTA. The carbon-encapsulated nanoparticles are superparamagnetic with the maximum saturation magnetization of 20 emu/g. This autothermal process has inherent advantages, including the use of low cost materials and the simplicity of the production protocol.

引用

页码：217 / 230

页数：14

共 22 条

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