Synthesis and magnetic properties of glass-ceramic composites SrFe12O19-SrSiO3

被引:17
作者
Zaitsev, DD
Kazin, PE
Tretyakov, YD
Jansen, M
机构
[1] Moscow MV Lomonosov State Univ, Dept Mat Sci, Moscow 119992, Russia
[2] Moscow MV Lomonosov State Univ, Dept Chem, Moscow 119992, Russia
[3] Max Planck Inst Festkorperforsch, D-70569 Stuttgart, Germany
基金
俄罗斯基础研究基金会;
关键词
Sr-ferrite; glass-cerarnics; magnetic properties;
D O I
10.1016/j.jmmm.2004.10.095
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Samples of magnetic glass-ceramics SrFe12P19-SrSiO3 were obtained by a heat treatment of the oxide glass at temperatures of 700-1250 degrees C. The materials were investigated using XRD analysis, magnetic measurements, electronic microcopy, Mossbauer spectroscopy, and thermal analysis. The magnetic phase started to develop at 700 degrees C and the fully crystalline SrFe12O19-SrSiO3 material formed at 1000 degrees C. The particles of SrFe12O19 phase demonstrated plate-like shape with the size and aspect ratio dependent on the thermal treatment conditions. The coercive force of the samples synthesized at 700-950 degrees C increased sharply from low values to 4700 Oe, and for samples prepared at higher temperatures it reached 5050 Oe. (c) 2004 Elsevier B.V. All rights reserved.
引用
收藏
页码:59 / 64
页数:6
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