Screening of antimony in PVC by solid sampling-graphite furnace atomic absorption spectrometry

被引:16
作者
Belarra, MA [1 ]
Belategui, I [1 ]
Lavilla, I [1 ]
Anzano, JM [1 ]
Castillo, JR [1 ]
机构
[1] Univ Zaragoza, Dept Analyt Chem, E-50009 Zaragoza, Spain
关键词
direct analysis; solid samples; antimony screening; graphite-furnace atomic absorption spectrometry;
D O I
10.1016/S0039-9140(97)00390-1
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
The development of two-stage control systems is of great interest when a large number of samples are analysed in order to check that they fulfil certain requirements. If the first stage is carried out using an inexpensive method with a high throughput which makes it possible to filter out the majority of the samples that fulfil the requirements, the procedure is not only less time-consuming but also more economical. Direct determination of metals in solid samples by graphite furnace atomic absorption spectrometry (GFAAS) appears, in principle, to be a suitable analytical technique for screening purposes since it provides sufficiently reliable results in a reasonably short time. In this paper it is applied with satisfactory results to antimony content control in a PVC sample. (C) 1998 Elsevier Science B.V. All rights reserved.
引用
收藏
页码:1265 / 1272
页数:8
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