[1] Ecole Natl Ingn Sfax, Unite Anal Alimentaires, Sfax 3038, Tunisia
[2] Ecole Natl Ingn Sfax, Lab Chim Ind, Sfax 3038, Tunisia
[3] Fac Univ Sci Agron Gembloux, Unite Chim Biol Ind, B-5030 Gembloux, Belgium
[4] Fac Sci Agron Etat Gembloux, Unite Technol Ind Agroalimentaires, B-5030 Gembloux, Belgium