Simultaneous measurement of 1H-15N, 1H-13C′, and 15N-13C′ dipolar couplings in a perdeuterated 30 kDa protein dissolved in a dilute liquid crystailine phase

被引：69

作者：

Wang, YX

Marquardt, JL

Wingfield, P

Stahl, SJ

Lee-Huang, S

Torchia, D

Bax, A ^{[1
]}

机构：

[1] NIDDKD, Chem Phys Lab, NIH, Bethesda, MD 20892 USA

[2] NIAMSD, Prot Express Lab, NIH, Bethesda, MD 20892 USA

[3] NIDR, Mol Struct Biol Unit, NIH, Bethesda, MD 20892 USA

[4] NYU, Sch Med, Dept Biochem, New York, NY 10016 USA

来源：

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY | 1998年 / 120卷 / 29期

关键词：

D O I：

10.1021/ja980862o

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

引用

页码：7385 / 7386

页数：2

共 24 条

[1]

Bastiaan E. W., 1987, ANNU REP NMR SPECTRO, V19, P35

[2] High-resolution heteronuclear NMR of human ubiquitin in an aqueous liquid crystalline medium [J].

Bax, A ;

Tjandra, N .

JOURNAL OF BIOMOLECULAR NMR, 1997, 10 (03) :289-292

[3] Protein phi and psi dihedral restraints determined from multidimensional hypersurface correlations of backbone chemical shifts and their use in the determination of protein tertiary structures [J].

Beger, RD ;

Bolton, PH .

JOURNAL OF BIOMOLECULAR NMR, 1997, 10 (02) :129-142

[4]

Bothner-By A. A., 1996, ENCY NUCL MAGNETIC R, P2932

[5] A robust method for determining the magnitude of the fully asymmetric alignment tensor of oriented macromolecules in the absence of structural information [J].

Clore, GM ;

Gronenborn, AM ;

Bax, A .

JOURNAL OF MAGNETIC RESONANCE, 1998, 133 (01) :216-221

[6]

DROBNY G, 1983, NUCL MAGNETIC RESONA, P289

[7] INTERFERENCE EFFECTS IN THE RELAXATION OF A PAIR OF UNLIKE SPIN-1/2 NUCLEI [J].

GOLDMAN, M .

JOURNAL OF MAGNETIC RESONANCE, 1984, 60 (03) :437-452

[8]

GRZESIEK S, 1995, J AM CHEM SOC, V117, P9596

[9] Solution NMR spectroscopy beyond 25 kDa [J].

Kay, LE ;

Gardner, KH .

CURRENT OPINION IN STRUCTURAL BIOLOGY, 1997, 7 (05) :722-731

[10]

Lindon JC., 1975, NMR SPECTROSCOPY USI

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