High-resolution 1H NMR spectroscopy in the solid state:: Very fast sample rotation and multiple-quantum coherences

被引：305

作者：

Schnell, I ^{[1
]}

Spiess, HW ^{[1
]}

机构：

[1] Max Planck Inst Polymer Res, D-55021 Mainz, Germany

来源：

JOURNAL OF MAGNETIC RESONANCE | 2001年 / 151卷 / 02期

关键词：

proton solid-state NMR; fast magic-angle spinning; multiple-quantum spectroscopy;

D O I：

10.1006/jmre.2001.2336

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

In the past few years, solid-state H-1 NMR spectroscopy under fast magic-angle spinning (MAS) has developed into a versatile tool for elucidating structure and dynamics. Dipolar multiple-quantum (MQ), in particular double-quantum (DQ), MAS spectroscopy has been applied to a variety of materials and provided unique insight, e.g., into the structure of hydrogen-bonded systems. This review intends to present solid-state H-1 DQ and MQ MAS spectroscopy in a systematic fashion with a particular emphasis on methodological aspects, followed by an overview of applications. (C) 2001 Academic Press.

引用

页码：153 / 227

页数：75

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