Wall thickness and core radius determination in surfactant templated silica thin films using GISAXS and X-ray reflectivity

被引:34
作者
Gibaud, A [1 ]
Baptiste, A
Doshi, DA
Brinker, CJ
Yang, L
Ocko, B
机构
[1] Univ Maine, Fac Sci, F-72085 Le Mans 09, France
[2] Univ New Mexico, Albuquerque, NM 87106 USA
[3] Sandia Natl Labs, Albuquerque, NM 87185 USA
[4] Brookhaven Natl Lab, Upton Long Isl, NY 11987 USA
来源
EUROPHYSICS LETTERS | 2003年 / 63卷 / 06期
关键词
D O I
10.1209/epl/i2003-00596-9
中图分类号
O4 [物理学];
学科分类号
0702 ;
摘要
X-ray reflectometry and GISAXS (grazing angle small angle scattering) are combined to investigate the morphology and structural parameters of a surfactant templated 2D hexagonal thin-film silica mesophase. It is shown that X-ray reflectivity measurements contain invaluable information about the radius of the cylindrical rods and the distance between their cores. The reflectivity data are analyzed using a model of the electron density and combined with GISAXS measurements to derive the silica wall thickness.
引用
收藏
页码:833 / 839
页数:7
相关论文
共 36 条
[1]  
Baskaran S, 2000, ADV MATER, V12, P291, DOI 10.1002/(SICI)1521-4095(200002)12:4<291::AID-ADMA291>3.0.CO
[2]  
2-P
[3]   A new 3D organization of mesopores in oriented CTAB silica films [J].
Besson, S ;
Ricolleau, C ;
Gacoin, T ;
Jacquiod, C ;
Boilot, JP .
JOURNAL OF PHYSICAL CHEMISTRY B, 2000, 104 (51) :12095-12097
[4]  
Brinker CJ, 1999, ADV MATER, V11, P579, DOI 10.1002/(SICI)1521-4095(199905)11:7<579::AID-ADMA579>3.0.CO
[5]  
2-R
[6]  
BRINKER CJ, 1990, SOL GEL SCI PHYSICS
[7]   Properties of an electrochemically deposited Pb monolayer on Cu(111) [J].
Chu, YS ;
Robinson, IK ;
Gewirth, AA .
PHYSICAL REVIEW B, 1997, 55 (12) :7945-7954
[8]   A new application of UV-ozone treatment in the preparation of substrate-supported, mesoporous thin films [J].
Clark, T ;
Ruiz, JD ;
Fan, HY ;
Brinker, CJ ;
Swanson, BI ;
Parikh, AN .
CHEMISTRY OF MATERIALS, 2000, 12 (12) :3879-3884
[9]   Optically, defined multifunctional patterning of photosensitive thin-film silica mesophases [J].
Doshi, DA ;
Huesing, NK ;
Lu, MC ;
Fan, HY ;
Lu, YF ;
Simmons-Potter, K ;
Potter, BG ;
Hurd, AJ ;
Brinker, CJ .
SCIENCE, 2000, 290 (5489) :107-111
[10]   Self-assembled aerogel-like low dielectric constant films [J].
Fan, HY ;
Bentley, HR ;
Kathan, KR ;
Clem, P ;
Lu, YF ;
Brinker, CJ .
JOURNAL OF NON-CRYSTALLINE SOLIDS, 2001, 285 (1-3) :79-83