Improved multiplicity-edited ADEQUATE experiments

被引：16

作者：

Parella, T ^{[1
]}

Sánchez-Ferrando, F

机构：

[1] Univ Autonoma Barcelona, Fac Ciencies, Serv Ressonancia Magnet Nucl, E-08193 Bellaterra, Barcelona, Spain

[2] Univ Autonoma Barcelona, Fac Ciencies, Dept Quim, E-08193 Bellaterra, Barcelona, Spain

来源：

JOURNAL OF MAGNETIC RESONANCE | 2004年 / 166卷 / 01期

关键词：

NMR; adequate; carbon multiplicity; 2D NMR;

D O I：

10.1016/j.jmr.2003.10.010

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

A very simple strategy is proposed to extract carbon multiplicity information along with the classic knowledge of carbon-carbon connectivities in ADEQUATE experiments without affecting the sensitivity ratios of the original pulse schemes. These new multiplicity-edited ADEQUATE experiments prove to be highly helpful for complete H-1 and C-13 resonance assignment and also for automated and easy spin system characterization of samples at natural abundance, using a single NMR experiment. (C) 2003 Elsevier Inc. All rights reserved.

引用

页码：123 / 128

页数：6

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