High-resolution X-ray diffraction beamline at the LNLS for the study of charge, orbital and magnetic structures

被引:37
作者
Giles, C [1 ]
Yokaichiya, F
Kycia, SW
Sampaio, LC
Ardiles-Saravia, DC
Franco, MKK
Neuenschwander, RT
机构
[1] Univ Estadual Campinas, Inst Fis, BR-13081970 Campinas, SP, Brazil
[2] Lab Nacl Luz Sincrotron, Campinas, SP, Brazil
[3] CBPF, Rio De Janeiro, Brazil
关键词
X-ray magnetic scattering; beamline optics; instrumentation;
D O I
10.1107/S0909049503020958
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
A high-resolution X-ray diffraction beamline at the Brazilian Synchrotron Light Laboratory (LNLS) has been commissioned for the study of crystalline magnetic materials. The beamline optics is based on a Rh-coated vertical-focusing X-ray mirror and a sagittal-focusing double-crystal monochromator. The primary instrument is a six-circle diffractometer equipped with energy and polarization analysers and a closed-cycle He cryostat. The beamline source is a bending magnet of the 1.37 GeV storage ring of the LNLS, delivering approximately 4 x 10(10) photons s(-1) at 8 keV at the sample position. Resonant and non-resonant scattering are the main techniques used to study charge, orbital and magnetic structures. Examples of magnetic scattering in Ho and NiO single crystals, as well as orbital ordering in manganites thin films, are presented.
引用
收藏
页码:430 / 434
页数:5
相关论文
共 18 条
[1]   Structural investigation of the dynamics of the NiO(111) surface by GIXS [J].
Barbier, A ;
Renaud, G ;
Mocuta, C ;
Stierle, A .
SURFACE SCIENCE, 1999, 433 :761-764
[2]  
*CERT SCI SOFTW, 1992, SPEC
[3]   A 2-CRYSTAL MONOCHROMATOR FOR THE UVX RING OF LNLS [J].
CORREA, MC ;
TOLENTINO, H ;
CRAIEVICH, A ;
CUSATIS, C .
REVIEW OF SCIENTIFIC INSTRUMENTS, 1992, 63 (01) :896-898
[4]   OBSERVATION OF MAGNETIC SUPERLATTICE PEAKS BY X-RAY-DIFFRACTION ON AN ANTIFERROMAGNETIC NIO CRYSTAL [J].
DEBERGEVIN, F ;
BRUNEL, M .
PHYSICS LETTERS A, 1972, A 39 (02) :141-+
[5]   Observation of orbital moment in NiO [J].
Fernandez, V ;
Vettier, C ;
de Bergevin, F ;
Giles, C ;
Neubeck, W .
PHYSICAL REVIEW B, 1998, 57 (13) :7870-7876
[6]   POLARIZATION AND RESONANCE PROPERTIES OF MAGNETIC-X-RAY SCATTERING IN HOLMIUM [J].
GIBBS, D ;
HARSHMAN, DR ;
ISAACS, ED ;
MCWHAN, DB ;
MILLS, D ;
VETTIER, C .
PHYSICAL REVIEW LETTERS, 1988, 61 (10) :1241-1244
[7]   First experiments on diffraction-enhanced imaging at LNLS [J].
Giles, C ;
Hönnicke, MG ;
Lopes, RT ;
Rocha, HS ;
Gonçalves, OD ;
Mazzaro, I ;
Cusatis, C .
JOURNAL OF SYNCHROTRON RADIATION, 2003, 10 :421-423
[8]  
GRANADO E, 2003, XRD2156502 LNLS RES
[9]   K-edge resonant x-ray magnetic scattering from a transition-metal oxide: NiO [J].
Hill, JP ;
Kao, CC ;
McMorrow, DF .
PHYSICAL REVIEW B, 1997, 55 (14) :R8662-R8665
[10]   Direct evaluation of composition profile, strain relaxation, and elastic energy of Ge:Si(001) self-assembled islands by anomalous x-ray scattering -: art. no. 245312 [J].
Magalhaes-Paniago, R ;
Medeiros-Ribeiro, G ;
Malachias, A ;
Kycia, S ;
Kamins, TI ;
Williams, RS .
PHYSICAL REVIEW B, 2002, 66 (24) :1-6