Three-dimensional imaging of crystal defects by 'topo-tomography'

被引:94
作者
Ludwig, W
Cloetens, P
Härtwig, J
Baruchel, J
Hamelin, B
Bastie, P
机构
[1] European Synchrotron Radiat Facil, F-38043 Grenoble, France
[2] Inst Max Von Laue Paul Langevin, F-38042 Grenoble 9, France
[3] Spectrometrie Phys Lab, F-38402 St Martin Dheres, France
关键词
D O I
10.1107/S002188980101086X
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
A new technique, 'topo-tomography', suitable for the characterization of the three-dimensional defect structure in bulk crystals, is proposed. The technique consists of the combination of diffraction topography and microtomography. It is applicable to high-quality single crystals, provided that the 'direct image' is the dominant contrast mechanism. In this case, crystal defects give rise to locally enhanced intensity compared with the perfect-crystal matrix. The additional intensities sum along the diffracted-beam direction and yield projections of the local Bragg reflectivity. Like in the case of absorption tomography, the three-dimensional distribution of this reflectivity can be reconstructed from a large number of projections. The first experimental results of this technique, applied to a synthetic diamond crystal, are presented.
引用
收藏
页码:602 / 607
页数:6
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