A nanoindentation study of copper films on oxidised silicon substrates

被引:89
作者
Beegan, D
Chowdhury, S
Laugier, MT [1 ]
机构
[1] Univ Limerick, Dept Phys, Limerick, Ireland
[2] Univ Limerick, Mat & Surface Sci Inst, Limerick, Ireland
关键词
nanoindentation; atomic force microscopy (AFM); copper;
D O I
10.1016/S0257-8972(03)00774-6
中图分类号
TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
The indentation hardness of copper films deposited on oxidised silicon substrates is investigated by two methods. The first uses the Oliver and Pharr method for analysing the load-displacement curves and the second involves the measurement of the residual indent impression with AFM. Material pile-up was found at the indent edges, and this area needs to be accounted for in hardness measurement. The effect of the pile-up area is investigated and the 'true' film hardness is determined. (C) 2003 Elsevier B.V. All rights reserved.
引用
收藏
页码:124 / 130
页数:7
相关论文
共 18 条
[1]   Finite element studies of the influence of pile-up on the analysis of nanoindentation data [J].
Bolshakov, A ;
Oliver, WC ;
Pharr, GM .
THIN FILMS: STRESSES AND MECHANICAL PROPERTIES VI, 1997, 436 :141-146
[2]   Numerical study on the measurement of thin film mechanical properties by means of nanoindentation [J].
Chen, X ;
Vlassak, JJ .
JOURNAL OF MATERIALS RESEARCH, 2001, 16 (10) :2974-2982
[3]   A method for interpreting the data from depth-sensing indentation instruments [J].
Doerner, M. F. ;
Nix, W. D. .
JOURNAL OF MATERIALS RESEARCH, 1986, 1 (04) :601-609
[4]   A review of analysis methods for sub-micron indentation testing [J].
Fischer-Cripps, AC .
VACUUM, 2000, 58 (04) :569-585
[5]   Substrate effects on indentation plastic zone development in thin soft films [J].
Kramer, DE ;
Volinsky, AA ;
Moody, NR ;
Gerberich, WW .
JOURNAL OF MATERIALS RESEARCH, 2001, 16 (11) :3150-3157
[6]  
Lucas BN, 1997, MATER RES SOC SYMP P, V436, P233
[7]   Test rate effects on the mechanical behavior of thin aluminum films [J].
Moody, NR ;
Strojny, A ;
Medlin, D ;
Guthrie, S ;
Gerberich, WW .
FUNDAMENTALS OF NANOINDENTATION AND NANOTRIBOLOGY, 1998, 522 :281-286
[8]   Indentation size effects in crystalline materials: A law for strain gradient plasticity [J].
Nix, WD ;
Gao, HJ .
JOURNAL OF THE MECHANICS AND PHYSICS OF SOLIDS, 1998, 46 (03) :411-425
[9]   AN IMPROVED TECHNIQUE FOR DETERMINING HARDNESS AND ELASTIC-MODULUS USING LOAD AND DISPLACEMENT SENSING INDENTATION EXPERIMENTS [J].
OLIVER, WC ;
PHARR, GM .
JOURNAL OF MATERIALS RESEARCH, 1992, 7 (06) :1564-1583
[10]   Measurement of mechanical properties by ultra-low load indentation [J].
Pharr, GM .
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 1998, 253 (1-2) :151-159