Synthesis of phosphorylated methanofullerenes

被引：13

作者：

Nuretdinov, IA ^{[1
]}

Gubskaya, VP ^{[1
]}

Berezhnaya, LS ^{[1
]}

Il'yasov, AV ^{[1
]}

Azancheev, NM ^{[1
]}

机构：

[1] Russian Acad Sci, Kazan Res Ctr, AE Arbuzov Organ & Phys Chem Inst, Kazan 420088, Russia

来源：

RUSSIAN CHEMICAL BULLETIN | 2000年 / 49卷 / 12期

关键词：

fullerene C-60; the Bingel reaction; 61-alkoxycarbonyl-61-(dimethoxyphosphoryl)methanofullerenes; UV and IR spectroscopy; H-1; C-13; and P-31 NMR spectroscopy;

D O I：

10.1023/A:1009584211531

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The reactions of fullerene C-60 with bromo(dimethoxyphosphoryl) acetates in the presence of NaH in toluene afforded alkoxycarbonyl(dimethoxyphosphoryl)methanofullerenes whose structures were established by UV, IR, and H-1, C-13, and P-31 NMR spectroscopy.

引用

页码：2048 / 2050

页数：3

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