Solvo-thermal synthesis of crystalline dinickel phosphide

被引：8

作者：

Lü, B

Bai, YJ

Feng, X

Zhao, YR

Yang, J

Chi, JR

机构：

[1] Shandong Univ Sci & Technol, Dept Mech Engn, Jinan 250031, Peoples R China

[2] Qingdao Univ, Coll Mech Engn, Qingdao 266071, Peoples R China

来源：

JOURNAL OF CRYSTAL GROWTH | 2004年 / 260卷 / 1-2期

关键词：

solvents; X-ray diffraction; nanomaterials; phosphides;

D O I：

10.1016/j.jcrysgro.2003.08.003

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

Nanocrystalline dinickel phosphide was synthesized via a solvo-thermal route using PCl3 and NiCl2 as precursors, and Na as reductant. The crystals were characterized by X-ray powder diffraction and transmission electronic microscopy. It was shown that the product is pure Ni2P which crystallizes very well with an average size of about 80 nm. (C) 2003 Elsevier B.V. All rights reserved.

引用

页码：115 / 117

页数：3

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