Hydrothermal preparation and characterization of Zn2SnO4 particles

被引：57

作者：

Fang, J

Huang, AH

Zhu, PX

Xu, NS

Xie, JQ

Chi, JS

Feng, SH

Xu, RR

Wu, MM ^{[1
]}

机构：

[1] Zhongshan Univ, Dept Chem, State Key Lab Ultrafast Laser & Spectroscopy, Guangzhou 510275, Peoples R China

[2] Jilin Univ, Key Lab Inorgan Synth & Preparat Chem, Changchun 130023, Peoples R China

来源：

MATERIALS RESEARCH BULLETIN | 2001年 / 36卷 / 7-8期

基金：

中国国家自然科学基金;

关键词：

inorganic compounds; oxides; chemical synthesis;

D O I：

10.1016/S0025-5408(01)00621-3

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

A phase-pure A(2)(II)B(IV)O(4)-typed complex oxide with spinel structure, Zn2SnO4 was synthesized via hydrothermal method under much milder conditions as compared to conventional solid-state reaction carried out at over 1000 degreesC. The influence of reaction conditions such as concentrations of mineralizer, reaction temperatures, and reaction times on the formation of Zn2SnO4 was described. The adoption of different inorganic zinc and/or tin sources still led to the almost same granular morphology of Zn2SnO4 particles. (C) 2001 Elsevier Science Ltd. All rights reserved.

引用

页码：1391 / 1397

页数：7

共 21 条

[1] Absence of the Coulomb gap at the Fermi level in the variable-range hopping regime of zinc stannate polycrystalline systems [J].