Automation of radiochemical analysis by flow injection techniques:: Am-Pu separation using TRU-resin™ sorbent extraction column

被引:25
作者
Egorov, O
Grate, JW
Ruzicka, J
机构
[1] Pacific NW Lab, Environm Mol Sci Lab, Richland, WA 99352 USA
[2] Univ Washington, Dept Chem, Seattle, WA 98195 USA
关键词
D O I
10.1007/BF02389777
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
A rapid automated flow injection analysis (FIA) procedure was developed for efficient separation of Am and Pu from each other and from interfering matrix and radionuclide components using a TRU-resin(TM)column. Selective Pu elution is enabled via on-column reduction. The separation was developed using on-line radioactivity detection. After the separation had been developed, fraction collection was used to obtain the separated fractions. In this manner, a FIA instrument functions as an automated separation workstation capable of unattended operation.
引用
收藏
页码:231 / 235
页数:5
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