Dipolar recoupling in MAS spectra of biological solids

被引：295

作者：

Griffin, RG ^{[1
]}

机构：

[1] MIT, Francis Bitter Natl Magnet Lab, Cambridge, MA 02139 USA

[2] MIT, Dept Chem, Cambridge, MA 02139 USA

来源：

NATURE STRUCTURAL BIOLOGY | 1998年 / 5卷 / Suppl 7期

关键词：

D O I：

10.1038/749

中图分类号：

Q5 [生物化学]; Q7 [分子生物学];

学科分类号：

071010 ; 081704 ;

摘要：

In combination with magic angle spinning, dipolar recoupling yields solid state NMR spectral assignments and provides constraints on internuclear distances and torsion angles. The method offers a fresh approach to structural studies of a variety of systems that cannot be examined with conventional tools available to structural biology.

引用

页码：508 / 512

页数：5

共 53 条

[1] NUCLEAR MAGNETIC RESONANCE SPECTRA FROM A CRYSTAL ROTATED AT HIGH SPEED [J].

ANDREW, ER ;

BRADBURY, A ;

EADES, RG .

NATURE, 1958, 182 (4650) :1659-1659

[2] CP-MAS C-13-NMR DIPOLAR CORRELATION SPECTROSCOPY OF C-13-ENRICHED CHLOROSOMES AND ISOLATED BACTERIOCHLOROPHYLL-C AGGREGATES OF CHLOROBIUM-TEPIDUM - THE SELF-ORGANIZATION OF PIGMENTS IS THE MAIN STRUCTURAL FEATURE OF CHLOROSOMES [J].

BALABAN, TS ;

HOLZWARTH, AR ;

SCHAFFNER, K ;

BOENDER, GJ ;

DEGROOT, HJM .

BIOCHEMISTRY, 1995, 34 (46) :15259-15266

[3] Efficient N-15-C-13 polarization transfer by adiabatic-passage Hartmann-Hahn cross polarization [J].

Baldus, M ;

Geurts, DG ;

Hediger, S ;

Meier, BH .

JOURNAL OF MAGNETIC RESONANCE SERIES A, 1996, 118 (01) :140-144

[4] BROAD-BAND POLARIZATION-TRANSFER EXPERIMENTS FOR ROTATING SOLIDS [J].

BALDUS, M ;

TOMASELLI, M ;

MEIER, BH ;

ERNST, RR .

CHEMICAL PHYSICS LETTERS, 1994, 230 (4-5) :329-336

[5] Homonuclear radio frequency-driven recoupling in rotating solids [J].

Bennett, AE ;

Rienstra, CM ;

Griffiths, JM ;

Zhen, WG ;

Lansbury, PT ;

Griffin, RG .

JOURNAL OF CHEMICAL PHYSICS, 1998, 108 (22) :9463-9479

[6] CHEMICAL-SHIFT CORRELATION SPECTROSCOPY IN ROTATING SOLIDS - RADIO FREQUENCY-DRIVEN DIPOLAR RECOUPLING AND LONGITUDINAL EXCHANGE [J].

BENNETT, AE ;

OK, JH ;

GRIFFIN, RG ;

VEGA, S .

JOURNAL OF CHEMICAL PHYSICS, 1992, 96 (11) :8624-8627

[7]

BENNETT AE, 1994, NMR-B PR PR, V33, P1

[8] MAS NMR STRUCTURE REFINEMENT OF UNIFORMLY C-13 ENRICHED CHLOROPHYLL-A WATER AGGREGATES WITH 2D DIPOLAR CORRELATION SPECTROSCOPY [J].

BOENDER, GJ ;

RAAP, J ;

PRYTULLA, S ;

OSCHKINAT, H ;

DEGROOT, HJM .

CHEMICAL PHYSICS LETTERS, 1995, 237 (5-6) :502-508

[9] Rotational resonance tickling: Accurate internuclear distance measurement in solids [J].

Costa, PR ;

Sun, BQ ;

Griffin, RG .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1997, 119 (44) :10821-10830

[10] Solid-state NMR measurement of Ψ in peptides:: a NCCN 2Q-heteronuclear local field experiment [J].

Costa, PR ;

Gross, JD ;

Hong, M ;

Griffin, RG .

CHEMICAL PHYSICS LETTERS, 1997, 280 (1-2) :95-103

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