Tenfold interpenetration of giant hexagonal R1212(126) nets in the hydrogen-bonded structure of 1,1,1-tris(4-hydroxyphenyl)ethane-4,4′-bipyridyl (2/3)

被引：21

作者：

Benyei, AC

Coupar, PI

Ferguson, G

Glidewell, C

Lough, AJ

Meehan, PR

机构：

[1] Lajos Kossuth Univ, Inst Phys Chem, H-4010 Debrecen, Hungary

[2] Univ St Andrews, Sch Chem, St Andrews KY16 9ST, Fife, Scotland

[3] Univ Guelph, Dept Chem & Biochem, Guelph, ON N1G 2W1, Canada

[4] Univ Toronto, Lash Miller Chem Labs, Toronto, ON M5S 3H6, Canada

来源：

ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS | 1998年 / 54卷

关键词：

D O I：

10.1107/S0108270198004624

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

In the 2:3 adduct of 1,1,1-tris(4-hydroxyphenyl)ethane [or ethane-1,1,1-triyltris(4-phenol)] and 4,4'-bipyridyl, 2C(20)H(18)O(3).3C(10)H(8)N(2), the components are linked by O-H ... N hydrogen bonds [N ... O 2.780(2), 2.745 (2) and 2.731(2)Angstrom] into puckered two-dimensional nets built from giant hexagons, each involving six units of each component. There are ten such independent nets, all multiply interwoven, within the structure.

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收藏

页码：1515 / 1519

页数：5

相关论文

共 22 条

[1] PATTERNS IN HYDROGEN BONDING - FUNCTIONALITY AND GRAPH SET ANALYSIS IN CRYSTALS [J].

BERNSTEIN, J ;

DAVIS, RE ;

SHIMONI, L ;

CHANG, NL .

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 1995, 34 (15) :1555-1573

[2] Crystal engineering using bisphenols and trisphenols. Complexes with hexamethylenetetramine (HMTA): Strings, multiple helices and chains-of-rings in the crystal structures of the adducts of HMTA with 4,4'-thiodiphenol(1/1), 4,4'-sulfonyldiphenol(1/1), 4,4'-isopropylidenediphenol(1/1), 1,1,1-tris(4-hydroxyphenyl)ethane(1/2) and 1,3,5-trihydroxybenzene(2/3) [J].

Coupar, PI ;

Glidewell, C ;

Ferguson, G .

ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE, 1997, 53 :521-533

[3] Pairwise-interwoven R66(48) hexagonal nets in the hydrogen-bonded structure of hexamethylenetetramine-1,1,1-tris(4-hydroxyphenyl)ethane (1/1) [J].

Coupar, PI ;

Ferguson, G ;

Glidewell, C ;

Meehan, PR .

ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1997, 53 :1978-1980

[4] Hydrogen-bonded chains in 4,4'-dihydroxybenzophenone-4,4'-bipyridyl (1/1) and chains of rings in 1,3,5-trihydroxylbenzene-4,4'-bipyridyl (2/3) [J].

Coupar, PI ;

Ferguson, G ;

Glidewell, C .

ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1996, 52 :2524-2528

[5] CRYSTAL STRUCTURE OF TRIMESIC ACID (BENZENE-1,3,5-TRICARBOXYLIC ACID) [J].

DUCHAMP, DJ ;

MARSH, RE .

ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL CRYSTALLOGRAPHY AND CRYSTAL CHEMISTRY, 1969, B 25 :5-&

[6] DISTORTED TRIPLE-DIAMOND STRUCTURE OF 3,3-BIS(CARBOXYMETHYL)GLUTARIC ACID (METHANETETRAACETIC ACID) [J].

ERMER, O ;

ELING, A .

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION IN ENGLISH, 1988, 27 (06) :829-833

[7] FIVEFOLD-DIAMOND STRUCTURE OF ADAMANTANE-1,3,5,7-TETRACARBOXYLIC ACID [J].

ERMER, O .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1988, 110 (12) :3747-3754

[8] ENCODING AND DECODING HYDROGEN-BOND PATTERNS OF ORGANIC-COMPOUNDS [J].

ETTER, MC .

ACCOUNTS OF CHEMICAL RESEARCH, 1990, 23 (04) :120-126

[9] Crystal engineering using trisphenols. Three-dimensional hydrogen-bonding networks in 1,1,1-tris(4-hydroxyphenyl)ethane, its hydrated adduct with 1,4-diazabicyclo[2.2.2]octane(1/1/1) and its adduct with piperazine(4/3) [J].

Ferguson, G ;

Bell, W ;

Coupar, PI ;

Glidewell, C .

ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE, 1997, 53 :534-543

[10] Crystal engineering using bisphenols. Chains, ladders and sheets formed by the adducts of 1,4-diazabicyclo[2.2.2]octane with bisphenols: Structures of adducts with 4,4'-isopropylidenediphenol(1/1), 4,4'-oxodiphenol(1/1) and 4,4'-thiodiphenol(1/1 and 2/1) [J].

Ferguson, G ;

Coupar, PI ;

Glidewell, C .

ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE, 1997, 53 :513-520