Hadamard NMR spectroscopy

被引:169
作者
Kupce, E
Nishida, T
Freeman, R
机构
[1] Univ Cambridge Jesus College, Cambridge CB5 8BL, England
[2] Varian Associates Inc, Eynsham, Oxon, England
[3] Biovitrum AB, Stockholm, Sweden
关键词
NMR spectroscopy; frequency-domain excitation; Fourier transform method; Hadamard spectroscopy; multi-dimensional NMR; COUPLING-CONSTANT MEASUREMENTS; RESONANCE; PULSES;
D O I
10.1016/S0079-6565(03)00022-0
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
Hadamard technique which can speed up data acquisition by orders of magnitude in nuclear magnetic resonance spectroscopy is discussed. Practical examples of two- and three-dimensional Hadamard spectroscopy are presented for small molecules and the proteins agitoxin and ubiquitin. Alternative schemes for fast multi-dimensional spectroscopy are reviewed.
引用
收藏
页码:95 / 122
页数:28
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