Application of cogwheel phase cycling to sideband manipulation experiments in solid-state NMR

被引:51
作者
Ivchenko, N
Hughes, CE
Levitt, MH [1 ]
机构
[1] Univ Southampton, Dept Chem, Southampton SO17 1BJ, Hants, England
[2] Max Planck Inst Biophys Chem, D-37077 Gottingen, Germany
基金
英国工程与自然科学研究理事会;
关键词
cogwheel phase cycling; spinning sidebands; TOSS; PASS;
D O I
10.1016/S1090-7807(03)00206-4
中图分类号
Q5 [生物化学];
学科分类号
071010 ; 081704 ;
摘要
Cogwheel phase-cycling schemes are applied to sideband suppression and sideband separation experiments in solid-state NMR. It is shown that cogwheel phase cycles lead to the elimination of most pulse imperfection effects, while using far fewer experimental signal acquisitions than conventional phase-cycling methods. (C) 2003 Elsevier Inc. All rights reserved.
引用
收藏
页码:286 / 293
页数:8
相关论文
共 38 条
[1]   Sideband manipulation in magic-angle-spinning nuclear magnetic resonance [J].
Antzutkin, ON .
PROGRESS IN NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY, 1999, 35 (03) :203-266
[2]   SUPPRESSION OF SIDE-BAND IN MAGIC-ANGLE-SPINNING NUCLEAR-MAGNETIC-RESONANCE - GENERAL-PRINCIPLES AND ANALYTICAL SOLUTIONS [J].
ANTZUTKIN, ON ;
SONG, ZY ;
FENG, XL ;
LEVITT, MH .
JOURNAL OF CHEMICAL PHYSICS, 1994, 100 (01) :130-140
[3]   13C and 15N chemical shift anisotropy of ampicillin and penicillin-V studied by 2D-PASS and CP/MAS NMR [J].
Antzutkin, ON ;
Lee, YK ;
Levitt, MH .
JOURNAL OF MAGNETIC RESONANCE, 1998, 135 (01) :144-155
[4]   2-DIMENSIONAL SIDE-BAND SEPARATION IN MAGIC-ANGLE-SPINNING NMR [J].
ANTZUTKIN, ON ;
SHEKAR, SC ;
LEVITT, MH .
JOURNAL OF MAGNETIC RESONANCE SERIES A, 1995, 115 (01) :7-19
[5]   Multiple-rotor-cycle QPASS pulse sequences:: Separation of quadrupolar spinning sidebands with an application to 139La NMR [J].
Aurentz, DJ ;
Vogt, FG ;
Mueller, KT ;
Benesi, AJ .
JOURNAL OF MAGNETIC RESONANCE, 1999, 138 (02) :320-325
[6]  
Bain A.D., 1984, J MAGN RESON, V56, P418
[7]   SELECTION OF COHERENCE-TRANSFER PATHWAYS IN NMR PULSE EXPERIMENTS [J].
BODENHAUSEN, G ;
KOGLER, H ;
ERNST, RR .
JOURNAL OF MAGNETIC RESONANCE, 1984, 58 (03) :370-388
[8]   Two-dimensional MAS-NMR spectra which correlate fast and slow magic angle spinning sideband patterns [J].
Crockford, C ;
Geen, H ;
Titman, JJ .
CHEMICAL PHYSICS LETTERS, 2001, 344 (3-4) :367-373
[9]  
DELACROIX SF, 1992, J MAGN RESON, V97, P435