Magnetic nanoparticles and nanoparticle assemblies from metallorganic precursors

被引:29
作者
Gun'ko, YK [1 ]
Pillai, SC [1 ]
McInerney, D [1 ]
机构
[1] Univ Dublin Trinity Coll, Dept Chem, Dublin 2, Ireland
关键词
Atomic force microscopy - Condensation reactions - Heat treatment - Hydrolysis - Magnetite - Organometallics - Scanning electron microscopy - Transmission electron microscopy - Ultrasonic applications - X ray powder diffraction;
D O I
10.1023/A:1011284009174
中图分类号
TM [电工技术]; TN [电子技术、通信技术];
学科分类号
0808 ; 0809 ;
摘要
Magnetic nanoparticles of gamma -Fe2O3, Fe2O3/SiO2 composite and magnetite (Fe3O4) have been prepared using novel metallorganic precursors (Fe[NC(C6H4)C(NSiMe3)(2)](2)Cl, Fe-2[O2Si(C6H5)(2)](3) and [Fe(OBut)(3)Na(THF)](2)) by hydrolysis, sol-gel condensation and further ultrasound and thermal treatment of the samples. The nanoparticles have been investigated by X-ray powder diffraction, TEM, SEM and AFM. (C) 2001 Kluwer Academic Publishers.
引用
收藏
页码:299 / 302
页数:4
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