Magnetic nanoparticles and nanoparticle assemblies from metallorganic precursors

被引：29

作者：

Gun'ko, YK ^{[1
]}

Pillai, SC ^{[1
]}

McInerney, D ^{[1
]}

机构：

[1] Univ Dublin Trinity Coll, Dept Chem, Dublin 2, Ireland

来源：

JOURNAL OF MATERIALS SCIENCE-MATERIALS IN ELECTRONICS | 2001年 / 12卷 / 4-6期

关键词：

Atomic force microscopy - Condensation reactions - Heat treatment - Hydrolysis - Magnetite - Organometallics - Scanning electron microscopy - Transmission electron microscopy - Ultrasonic applications - X ray powder diffraction;

D O I：

10.1023/A:1011284009174

中图分类号：

TM [电工技术]; TN [电子技术、通信技术];

学科分类号：

0808 ; 0809 ;

摘要：

Magnetic nanoparticles of gamma -Fe2O3, Fe2O3/SiO2 composite and magnetite (Fe3O4) have been prepared using novel metallorganic precursors (Fe[NC(C6H4)C(NSiMe3)(2)](2)Cl, Fe-2[O2Si(C6H5)(2)](3) and [Fe(OBut)(3)Na(THF)](2)) by hydrolysis, sol-gel condensation and further ultrasound and thermal treatment of the samples. The nanoparticles have been investigated by X-ray powder diffraction, TEM, SEM and AFM. (C) 2001 Kluwer Academic Publishers.

引用

页码：299 / 302

页数：4