Simultaneous determination of anthraquinones, their 8-β-D-glucosides, and sennosides of Rhei rhizoma by capillary electrophoresis

被引:18
作者
Koyama, J [1 ]
Morita, I [1 ]
Fujiyoshi, H [1 ]
Kobayashi, N [1 ]
机构
[1] Kobe Pharmaceut Univ, Higashinada Ku, Kobe, Hyogo 6588558, Japan
关键词
cyclodextrin modified capillary zone electrophoresis; emodin; chrysophanol; rhein; sennoside; anthraquinone glucoside;
D O I
10.1248/cpb.53.573
中图分类号
R914 [药物化学];
学科分类号
100701 ;
摘要
The simultaneous separation and determination of major anthraquinones (emodin, chrysophanol, rhein and their glucosides, aloe-emodin, sennoside A, and sennoside B) of Rhei Rhizoma were achieved by cyclodextrin modified capillary zone electrophoresis. The running electrolyte used in this method was 0.005 M alpha-cyclodextrin in 0.03 M borate buffer (pH 10.0) containing 20% acetonitrile, with an applied voltage of 20 kV.
引用
收藏
页码:573 / 575
页数:3
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